4-((3-(3-chlorophenyl)imidazo[1,2-b]pyridazin-6-yl)amino)cyclohexanone oxime

Base Information

Chemical Name:4-((3-(3-chlorophenyl)imidazo[1,2-b]pyridazin-6-yl)amino)cyclohexanone oxime
CAS No.:1418142-85-4
Molecular Formula:C₁₈H₁₈ClN₅O
Molecular Weight:355.827
Hs Code.:

Synonyms:4-((3-(3-chlorophenyl)imidazo[1,2-b]pyridazin-6-yl)amino)cyclohexanone oxime

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Chemical Property of 4-((3-(3-chlorophenyl)imidazo[1,2-b]pyridazin-6-yl)amino)cyclohexanone oxime

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Technology Process of 4-((3-(3-chlorophenyl)imidazo[1,2-b]pyridazin-6-yl)amino)cyclohexanone oxime

There total 8 articles about 4-((3-(3-chlorophenyl)imidazo[1,2-b]pyridazin-6-yl)amino)cyclohexanone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 1418142-65-0
4-((3-(3-chlorophenyl)imidazo[1,2-b]pyridazin-6-yl)amino)cyclohexanone

: 1418142-85-4
4-((3-(3-chlorophenyl)imidazo[1,2-b]pyridazin-6-yl)amino)cyclohexanone oxime

Guidance literature:: With hydroxylamine hydrochloride; In methanol; at 0 - 20 ℃; for 1h;

Reference yield:

: 13526-66-4
3-bromo-6-chloro-imidazo[1,2-b]pyridazine

: 1418142-85-4
4-((3-(3-chlorophenyl)imidazo[1,2-b]pyridazin-6-yl)amino)cyclohexanone oxime

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 3 h / 110 °C

2: sodium hydrogencarbonate / 1-methyl-pyrrolidin-2-one / 1 h / 180 °C / Microwave irradiation

3: hydroxylamine hydrochloride / methanol / 1 h / 0 - 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydroxylamine hydrochloride; sodium hydrogencarbonate; potassium carbonate; In 1,4-dioxane; 1-methyl-pyrrolidin-2-one; methanol; water;

Reference yield:

: 63503-60-6
3-chlorophenylboronic acid

: 1418142-85-4
4-((3-(3-chlorophenyl)imidazo[1,2-b]pyridazin-6-yl)amino)cyclohexanone oxime

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 3 h / 110 °C

2: sodium hydrogencarbonate / 1-methyl-pyrrolidin-2-one / 1 h / 180 °C / Microwave irradiation

3: hydroxylamine hydrochloride / methanol / 1 h / 0 - 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydroxylamine hydrochloride; sodium hydrogencarbonate; potassium carbonate; In 1,4-dioxane; 1-methyl-pyrrolidin-2-one; methanol; water;