Formic acid (4aS,7S,7aS)-4a-((R)-4-methoxy-1-methyl-cyclohexa-2,4-dienyl)-hexahydro-cyclopenta[1,3]dioxin-7-yl ester

Base Information

• Chemical Name: Formic acid (4aS,7S,7aS)-4a-((R)-4-methoxy-1-methyl-cyclohexa-2,4-dienyl)-hexahydro-cyclopenta[1,3]dioxin-7-yl ester
• CAS No.: 77229-29-9
• Molecular Formula: C₁₆H₂₂O₅
• Molecular Weight: 294.348

Synonyms:Formic acid (4aS,7S,7aS)-4a-((R)-4-methoxy-1-methyl-cyclohexa-2,4-dienyl)-hexahydro-cyclopenta[1,3]dioxin-7-yl ester

Chemical Property of Formic acid (4aS,7S,7aS)-4a-((R)-4-methoxy-1-methyl-cyclohexa-2,4-dienyl)-hexahydro-cyclopenta[1,3]dioxin-7-yl ester

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Technology Process of Formic acid (4aS,7S,7aS)-4a-((R)-4-methoxy-1-methyl-cyclohexa-2,4-dienyl)-hexahydro-cyclopenta[1,3]dioxin-7-yl ester

There total 1 articles about Formic acid (4aS,7S,7aS)-4a-((R)-4-methoxy-1-methyl-cyclohexa-2,4-dienyl)-hexahydro-cyclopenta[1,3]dioxin-7-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

→ Formic acid (4aS,7S,7aS)-4a-((R)-4-methoxy-1-methyl-cyclohexa-2,4-dienyl)-hexahydro-cyclopenta[1,3]dioxin-7-yl ester (77229-29-9)

Guidance literature:

With trimethylamine-N-oxide; In benzene; at 50 ℃; for 3h;

DOI:10.1016/0040-4039(80)80095-5

Reference yield: 75.0%

Formic acid (4aS,7S,7aS)-4a-((R)-4-methoxy-1-methyl-cyclohexa-2,4-dienyl)-hexahydro-cyclopenta[1,3]dioxin-7-yl ester (77229-29-9) → Formic acid (4aS,7S,7aS)-4a-((R)-1-methyl-4-oxo-cyclohex-2-enyl)-hexahydro-cyclopenta[1,3]dioxin-7-yl ester (77229-30-2)

Guidance literature:

With oxalic acid; In methanol; water; at 0 ℃; for 0.5h;

DOI:10.1016/0040-4039(80)80095-5

Downstream raw materials:

Formic acid (4aS,7S,7aS)-4a-((R)-1-methyl-4-oxo-cyclohex-2-enyl)-hexahydro-cyclopenta[1,3]dioxin-7-yl ester

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