1-phthalimido-4-(N-benzyl)-8--11-amino-4,8-diazaundecane

Base Information

Chemical Name:1-phthalimido-4-(N-benzyl)-8--11-amino-4,8-diazaundecane
CAS No.:151915-09-2
Molecular Formula:C₄₄H₅₆N₄O₆S₂
Molecular Weight:801.084
Hs Code.:

1-phthalimido-4-(N-benzyl)-8-<N-(2-mesitylene)sulfonyl>-11-<N-ethyl-N-(2-mesitylene)sulfonyl>amino-4,8-diazaundecane

Synonyms:1-phthalimido-4-(N-benzyl)-8--11-amino-4,8-diazaundecane

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Chemical Property of 1-phthalimido-4-(N-benzyl)-8--11-amino-4,8-diazaundecane

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Technology Process of 1-phthalimido-4-(N-benzyl)-8--11-amino-4,8-diazaundecane

There total 6 articles about 1-phthalimido-4-(N-benzyl)-8--11-amino-4,8-diazaundecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 151915-08-1
N-ethyl-N-(3-iodopropyl)-(2-mesitylene)sulfonamide

: 151915-06-9
1-phthalimido-4-(N-benzyl)-7-<<(2-mesitylene)sulfonyl>amino>-4-azaheptane

: 151915-09-2
1-phthalimido-4-(N-benzyl)-8--11-amino-4,8-diazaundecane

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;
DOI:10.1021/jm00072a020

Reference yield:

: 773-64-8
2-mesitylenesulphonyl chloride

: 151915-09-2
1-phthalimido-4-(N-benzyl)-8--11-amino-4,8-diazaundecane

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / 10percent aq. NaOH / CH₂Cl₂ / 3 h / 0 - 20 °C

2: 1.) NaH / 1.) DMF, 0 deg C, 2.) DMF, THF, RT, 4 h

3: 96 percent / NaH / dimethylformamide / 0.5 h / 0 °C

With sodium hydroxide; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00072a020

Reference yield:

: 5460-29-7
2-(3-bromopropyl)isoindole-1,3-dione

: 151915-09-2
1-phthalimido-4-(N-benzyl)-8--11-amino-4,8-diazaundecane

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / Na₂CO₃, LiI / butan-1-ol / 24 h / 80 °C

2: 96 percent / NaH / dimethylformamide / 0.5 h / 0 °C

With sodium hydride; sodium carbonate; lithium iodide; In N,N-dimethyl-formamide; butan-1-ol;
DOI:10.1021/jm00072a020