(S)-2-tert-Butoxycarbonylamino-3-(4-hydroxy-3-iodo-phenyl)-propionic acid; compound with dicyclohexyl-amine

Base Information

Chemical Name:(S)-2-tert-Butoxycarbonylamino-3-(4-hydroxy-3-iodo-phenyl)-propionic acid; compound with dicyclohexyl-amine
CAS No.:73563-53-8
Molecular Formula:C₁₂H₂₃N*C₁₄H₁₈INO₅
Molecular Weight:588.526
Hs Code.:

Synonyms:(S)-2-tert-Butoxycarbonylamino-3-(4-hydroxy-3-iodo-phenyl)-propionic acid; compound with dicyclohexyl-amine

Suppliers and Price of (S)-2-tert-Butoxycarbonylamino-3-(4-hydroxy-3-iodo-phenyl)-propionic acid; compound with dicyclohexyl-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-2-tert-Butoxycarbonylamino-3-(4-hydroxy-3-iodo-phenyl)-propionic acid; compound with dicyclohexyl-amine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-2-tert-Butoxycarbonylamino-3-(4-hydroxy-3-iodo-phenyl)-propionic acid; compound with dicyclohexyl-amine

There total 5 articles about (S)-2-tert-Butoxycarbonylamino-3-(4-hydroxy-3-iodo-phenyl)-propionic acid; compound with dicyclohexyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 71400-63-0,478183-68-5
N-tert-butyloxycarbonyl-3-iodo-L-tyrosine

: 101-83-7
N-cyclohexyl-cyclohexanamine

: 73563-53-8
(S)-2-tert-Butoxycarbonylamino-3-(4-hydroxy-3-iodo-phenyl)-propionic acid; compound with dicyclohexyl-amine

Guidance literature:: In diethyl ether; at -5 ℃;
DOI:10.1002/jlac.198119810716

Reference yield:

: 1070-19-5
N-(tert-butyloxycarbonyl) azide

: 73563-53-8
(S)-2-tert-Butoxycarbonylamino-3-(4-hydroxy-3-iodo-phenyl)-propionic acid; compound with dicyclohexyl-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 1) NH₃ / 1) chloroform, 30 min, 2) pyridine, 4,5 days

2: 2 N NaOH / acetone / 2 h / Ambient temperature

3: 97 percent / diethyl ether / -5 °C

With sodium hydroxide; ammonia; In diethyl ether; acetone;
DOI:10.1002/jlac.198119810716

Reference yield:

: 70-78-0
3-Iodo-L-tyrosine

: 73563-53-8
(S)-2-tert-Butoxycarbonylamino-3-(4-hydroxy-3-iodo-phenyl)-propionic acid; compound with dicyclohexyl-amine

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / SOCl₂ / methanol / 41 h / 20 °C

2: 1) NH₃ / 1) chloroform, 30 min, 2) pyridine, 4,5 days

3: 2 N NaOH / acetone / 2 h / Ambient temperature

4: 97 percent / diethyl ether / -5 °C

With sodium hydroxide; thionyl chloride; ammonia; In methanol; diethyl ether; acetone;
DOI:10.1002/jlac.198119810716