C₂₁H₂₅FSi

Base Information

Chemical Name:C₂₁H₂₅FSi
CAS No.:1260426-14-9
Molecular Formula:C₂₁H₂₅FSi
Molecular Weight:324.513
Hs Code.:

Synonyms:C₂₁H₂₅FSi

Suppliers and Price of C₂₁H₂₅FSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₂₅FSi

Chemical Property:

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Technology Process of C₂₁H₂₅FSi

There total 4 articles about C₂₁H₂₅FSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1260426-18-3
C₂₆H₂₉NSi

: 1260426-14-9
C₂₁H₂₅FSi

Guidance literature:: With hydrogen fluoride; In tetrahydrofuran; water; at 0 - 20 ℃;
DOI:10.1002/adsc.201000975

Reference yield: 66.0%

: 1260426-13-8
C₁₃H₂₀FISi

: potassium (2-phenylethynyl)trifluoroborate

: 1260426-14-9
C₂₁H₂₅FSi

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; caesium carbonate; In tetrahydrofuran; for 48h; Inert atmosphere; Reflux;
DOI:10.1002/anie.201004426

Reference yield:

: 2227-29-4
chlorodiisopropylsilane

: 1260426-14-9
C₂₁H₂₅FSi

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / hexanes; diethyl ether / 0.67 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexanes / -78 °C / Inert atmosphere

2.2: -78 - 30 °C / Inert atmosphere

3.1: N-iodo-succinimide; [bis(acetoxy)iodo]benzene; palladium diacetate / 1,2-dichloro-ethane / 1 h / 70 °C / Inert atmosphere

4.1: hydrogen fluoride / tetrahydrofuran; water / 1 h / 20 °C

5.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; caesium carbonate / tetrahydrofuran / 48 h / Inert atmosphere; Reflux

With N-iodo-succinimide; n-butyllithium; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; [bis(acetoxy)iodo]benzene; hydrogen fluoride; palladium diacetate; caesium carbonate; In tetrahydrofuran; hexanes; diethyl ether; water; 1,2-dichloro-ethane;
DOI:10.1002/adsc.201000975