tert-butyl-{(1R,2S)-1-[2-(4-methoxybenzyloxy)ethyl]-2-[(4R,5S,6R)-2,2,5-trimethyl-6-((S)-1-methylbut-3-ynyl)-[1,3]dioxan-4-yl]propoxy}dimethylsilane

Base Information

Chemical Name:tert-butyl-{(1R,2S)-1-[2-(4-methoxybenzyloxy)ethyl]-2-[(4R,5S,6R)-2,2,5-trimethyl-6-((S)-1-methylbut-3-ynyl)-[1,3]dioxan-4-yl]propoxy}dimethylsilane
CAS No.:1185341-28-9
Molecular Formula:C₃₁H₅₂O₅Si
Molecular Weight:532.836
Hs Code.:

Synonyms:tert-butyl-{(1R,2S)-1-[2-(4-methoxybenzyloxy)ethyl]-2-[(4R,5S,6R)-2,2,5-trimethyl-6-((S)-1-methylbut-3-ynyl)-[1,3]dioxan-4-yl]propoxy}dimethylsilane

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Chemical Property of tert-butyl-{(1R,2S)-1-[2-(4-methoxybenzyloxy)ethyl]-2-[(4R,5S,6R)-2,2,5-trimethyl-6-((S)-1-methylbut-3-ynyl)-[1,3]dioxan-4-yl]propoxy}dimethylsilane

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Technology Process of tert-butyl-{(1R,2S)-1-[2-(4-methoxybenzyloxy)ethyl]-2-[(4R,5S,6R)-2,2,5-trimethyl-6-((S)-1-methylbut-3-ynyl)-[1,3]dioxan-4-yl]propoxy}dimethylsilane

There total 2 articles about tert-butyl-{(1R,2S)-1-[2-(4-methoxybenzyloxy)ethyl]-2-[(4R,5S,6R)-2,2,5-trimethyl-6-((S)-1-methylbut-3-ynyl)-[1,3]dioxan-4-yl]propoxy}dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1185341-70-1
toluene-4-sulfonic acid (S)-2-{(4R,5S,6R)-6-[(1S,2R)-2-(tert-butyldimethylsilanyloxy)-4-(4-methoxybenzyloxy)-1-methylbutyl]-2,2,5-trimethyl-[1,3]dioxan-4-yl}propyl ester

: 1066-26-8
sodium acetylide

: 1185341-28-9
tert-butyl-{(1R,2S)-1-[2-(4-methoxybenzyloxy)ethyl]-2-[(4R,5S,6R)-2,2,5-trimethyl-6-((S)-1-methylbut-3-ynyl)-[1,3]dioxan-4-yl]propoxy}dimethylsilane

Guidance literature:: In 5,5-dimethyl-1,3-cyclohexadiene; dimethyl sulfoxide; at 0 - 20 ℃;
DOI:10.1021/ja9056163

Reference yield: 72.0%

: 1185341-70-1
toluene-4-sulfonic acid (S)-2-{(4R,5S,6R)-6-[(1S,2R)-2-(tert-butyldimethylsilanyloxy)-4-(4-methoxybenzyloxy)-1-methylbutyl]-2,2,5-trimethyl-[1,3]dioxan-4-yl}propyl ester

: sodium acetylide

: 1185341-28-9
tert-butyl-{(1R,2S)-1-[2-(4-methoxybenzyloxy)ethyl]-2-[(4R,5S,6R)-2,2,5-trimethyl-6-((S)-1-methylbut-3-ynyl)-[1,3]dioxan-4-yl]propoxy}dimethylsilane

Guidance literature:: toluene-4-sulfonic acid (S)-2-{(4R,5S,6R)-6-[(1S,2R)-2-(tert-butyldimethylsilanyloxy)-4-(4-methoxybenzyloxy)-1-methylbutyl]-2,2,5-trimethyl-[1,3]dioxan-4-yl}propyl ester; sodium acetylide; In 5,5-dimethyl-1,3-cyclohexadiene; dimethyl sulfoxide; at 0 - 20 ℃;

With water; In 5,5-dimethyl-1,3-cyclohexadiene; dimethyl sulfoxide; at 20 ℃;
DOI:10.1021/jo100201f