3,3'-dimethyl-5,5'-triazene-1,3-diyl-bis-isothiazole-4-carboxylic acid diethyl ester

Base Information

Chemical Name:3,3'-dimethyl-5,5'-triazene-1,3-diyl-bis-isothiazole-4-carboxylic acid diethyl ester
CAS No.:24979-20-2
Molecular Formula:C₁₄H₁₇N₅O₄S₂
Molecular Weight:383.452
Hs Code.:

Synonyms:3,3'-dimethyl-5,5'-triazene-1,3-diyl-bis-isothiazole-4-carboxylic acid diethyl ester

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Chemical Property of 3,3'-dimethyl-5,5'-triazene-1,3-diyl-bis-isothiazole-4-carboxylic acid diethyl ester

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Technology Process of 3,3'-dimethyl-5,5'-triazene-1,3-diyl-bis-isothiazole-4-carboxylic acid diethyl ester

There total 2 articles about 3,3'-dimethyl-5,5'-triazene-1,3-diyl-bis-isothiazole-4-carboxylic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34859-65-9
ethyl 5-amino-3-methyl-isothiazole 4-carboxylate

: 4-ethoxycarbonyl-3-methyl-isothiazole-5-diazonium; tetrafluoroborate

: 24979-20-2
3,3'-dimethyl-5,5'-triazene-1,3-diyl-bis-isothiazole-4-carboxylic acid diethyl ester

Guidance literature:: In acetonitrile; at -10 ℃;

Reference yield:

: 34859-65-9
ethyl 5-amino-3-methyl-isothiazole 4-carboxylate

: 24979-20-2
3,3'-dimethyl-5,5'-triazene-1,3-diyl-bis-isothiazole-4-carboxylic acid diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaNO₂, aq. H₂SO₄

2: (heating in MeOH)

With sulfuric acid; sodium nitrite;