(rac)-ethyl [{3-[(4-{2-[(4-fluorobenzyl)oxy]phenyl}-1,3,5-triazin-2-yl)amino]benzyl}(methyl)oxido-λ6-sulfanylidene]carbamate

Base Information

Chemical Name:(rac)-ethyl [{3-[(4-{2-[(4-fluorobenzyl)oxy]phenyl}-1,3,5-triazin-2-yl)amino]benzyl}(methyl)oxido-λ6-sulfanylidene]carbamate
CAS No.:1415248-82-6
Molecular Formula:C₂₇H₂₆FN₅O₄S
Molecular Weight:535.599
Hs Code.:

Synonyms:(rac)-ethyl [{3-[(4-{2-[(4-fluorobenzyl)oxy]phenyl}-1,3,5-triazin-2-yl)amino]benzyl}(methyl)oxido-λ6-sulfanylidene]carbamate

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Chemical Property of (rac)-ethyl [{3-[(4-{2-[(4-fluorobenzyl)oxy]phenyl}-1,3,5-triazin-2-yl)amino]benzyl}(methyl)oxido-λ6-sulfanylidene]carbamate

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Technology Process of (rac)-ethyl [{3-[(4-{2-[(4-fluorobenzyl)oxy]phenyl}-1,3,5-triazin-2-yl)amino]benzyl}(methyl)oxido-λ6-sulfanylidene]carbamate

There total 8 articles about (rac)-ethyl [{3-[(4-{2-[(4-fluorobenzyl)oxy]phenyl}-1,3,5-triazin-2-yl)amino]benzyl}(methyl)oxido-λ6-sulfanylidene]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 870779-01-4
{2-[(4-fluorobenzyl)oxy]phenyl}boronic acid

: 1414944-24-3
(rac)-ethyl [{3-[(4-chloro-1,3,5-triazin-2-yl)amino]benzyl}(methyl)-oxido-λ⁶-sulfanylidene]carbamate

: 1415248-82-6
(rac)-ethyl [{3-[(4-{2-[(4-fluorobenzyl)oxy]phenyl}-1,3,5-triazin-2-yl)amino]benzyl}(methyl)oxido-λ6-sulfanylidene]carbamate

Guidance literature:: With potassium carbonate; [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II); In 1,2-dimethoxyethane; at 100 ℃; for 1.5h; Inert atmosphere;

Reference yield:

: 1414944-11-8
(rac)-1-[(methylsulfinyl)methyl]-3-nitrobenzene

: 1415248-82-6
(rac)-ethyl [{3-[(4-{2-[(4-fluorobenzyl)oxy]phenyl}-1,3,5-triazin-2-yl)amino]benzyl}(methyl)oxido-λ6-sulfanylidene]carbamate

Guidance literature:: Multi-step reaction with 6 steps

1.1: magnesium oxide; [bis(acetoxy)iodo]benzene / dirhodium tetraacetate / dichloromethane / 16 h / 20 °C

2.1: potassium carbonate; methanol / 1 h / 20 °C

3.1: pyridine / 24 h / 20 °C

4.1: hydrogenchloride; titanium(III) chloride / water; tetrahydrofuran / 18 h / 20 °C

4.2: pH 8 / Cooling with ice

5.1: N-ethyl-N,N-diisopropylamine / isopropyl alcohol; tetrahydrofuran / 3 h / -40 - 0 °C

6.1: potassium carbonate / [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II) / 1,2-dimethoxyethane / 1.5 h / 100 °C / Inert atmosphere

With pyridine; hydrogenchloride; methanol; titanium(III) chloride; [bis(acetoxy)iodo]benzene; magnesium oxide; potassium carbonate; N-ethyl-N,N-diisopropylamine; dirhodium tetraacetate; [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II); In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; isopropyl alcohol;

Reference yield:

: 619-23-8
3-Nitrobenzyl chloride

: 1415248-82-6
(rac)-ethyl [{3-[(4-{2-[(4-fluorobenzyl)oxy]phenyl}-1,3,5-triazin-2-yl)amino]benzyl}(methyl)oxido-λ6-sulfanylidene]carbamate

Guidance literature:: Multi-step reaction with 8 steps

1.1: ethanol / 3 h / -15 - 20 °C

2.1: periodic acid / iron(III) chloride / acetonitrile / 20 °C

3.1: magnesium oxide; [bis(acetoxy)iodo]benzene / dirhodium tetraacetate / dichloromethane / 16 h / 20 °C

4.1: potassium carbonate; methanol / 1 h / 20 °C

5.1: pyridine / 24 h / 20 °C

6.1: hydrogenchloride; titanium(III) chloride / water; tetrahydrofuran / 18 h / 20 °C

6.2: pH 8 / Cooling with ice

7.1: N-ethyl-N,N-diisopropylamine / isopropyl alcohol; tetrahydrofuran / 3 h / -40 - 0 °C

8.1: potassium carbonate / [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II) / 1,2-dimethoxyethane / 1.5 h / 100 °C / Inert atmosphere

With pyridine; hydrogenchloride; methanol; titanium(III) chloride; [bis(acetoxy)iodo]benzene; magnesium oxide; potassium carbonate; periodic acid; N-ethyl-N,N-diisopropylamine; iron(III) chloride; dirhodium tetraacetate; [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II); In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; dichloromethane; water; isopropyl alcohol; acetonitrile;