Ni-T(p-CO₂CH₃)PPCHO

Base Information

Chemical Name:Ni-T(p-CO₂CH₃)PPCHO
CAS No.:125824-99-9
Molecular Formula:C₅₃H₃₆N₄NiO₉
Molecular Weight:931.58
Hs Code.:

Ni-T(p-CO<sub>2</sub>CH<sub>3</sub>)PPCHO

Synonyms:Ni-T(p-CO₂CH₃)PPCHO

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Chemical Property of Ni-T(p-CO₂CH₃)PPCHO

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Technology Process of Ni-T(p-CO₂CH₃)PPCHO

There total 1 articles about Ni-T(p-CO₂CH₃)PPCHO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 58188-48-0
[5,10,15,20-tetrakis(4-methoxycarbonylphenyl)porphyrinato]-nickel(II)

: 125824-99-9
Ni-T(p-CO₂CH₃)PPCHO

Guidance literature:: With trichlorophosphate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; under reflux for 24 h, cooling down, addition of 10 % NaAc soln.; extn.(1,2-Cl2C2H4), washed with H2O, drying with MgSO4, evapn. under reduced pressure; chromy. (ethylacetate/toluene); elem. anal.;

Reference yield:

: 125824-99-9
Ni-T(p-CO₂CH₃)PPCHO

: t-butyloxycarbonylmethylene (triphenyl)phosphorane

: 125778-81-6,125827-65-8
cis-Ni-T(p-CO₂CH₃)PP-CH=CH-CO₂-t-Bu

: 125778-81-6,125827-65-8
trans-Ni-T(p-CO₂CH₃)PP-CH=CH-CO₂-t-Bu

Guidance literature:: In toluene; under reflux for 4 h, cooling down, concentrate under reduced pressure; sepn. by chromy.(Si, ethylene acetate/toluene: 1/9); elem. anal.;