C₄₄H₄₈ClN₃O₁₁Si

Base Information

Chemical Name:C₄₄H₄₈ClN₃O₁₁Si
CAS No.:1621966-46-8
Molecular Formula:C₄₄H₄₈ClN₃O₁₁Si
Molecular Weight:858.417
Hs Code.:

C<sub>44</sub>H<sub>48</sub>ClN<sub>3</sub>O<sub>11</sub>Si

Synonyms:C₄₄H₄₈ClN₃O₁₁Si

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Chemical Property of C₄₄H₄₈ClN₃O₁₁Si

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Technology Process of C₄₄H₄₈ClN₃O₁₁Si

There total 6 articles about C₄₄H₄₈ClN₃O₁₁Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 866605-99-4
(2R,3R,4R,5S,6S)-2-(acetoxymethyl)-6-(4-chloro-3-(hydroxymethyl)phenyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate

: 1613149-99-7
6-(((tert-butyldiphenylsilyl)oxy)methyl)-[1,2,4]triazolo[4,3-a]pyridin-3(2H)-one

: 1621966-46-8
C₄₄H₄₈ClN₃O₁₁Si

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃; for 15h; Inert atmosphere;
DOI:10.1016/j.bmc.2014.04.036

Reference yield:

: 866605-98-3
C₃₇H₄₃ClO₁₀Si

: 1621966-46-8
C₄₄H₄₈ClN₃O₁₁Si

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 15 h / 20 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; acetic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 2: |Mitsunobu Displacement;
DOI:10.1016/j.bmc.2014.04.036

Reference yield:

: 866605-96-1
(3R,4S,5S,6R)-2-(3-((tert-butyldiphenylsilyloxy)methyl)-4-chlorophenyl)-6-(hydroxymethyl)-2-methoxytetrahydro-2H-pyran-3,4,5-triol

: 1621966-46-8
C₄₄H₄₈ClN₃O₁₁Si

Guidance literature:: Multi-step reaction with 4 steps

1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 2 h / 0 °C

2: pyridine; dmap / chloroform / 20 °C

3: acetic acid; tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

4: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 15 h / 20 °C / Inert atmosphere

With pyridine; triethylsilane; dmap; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; acetic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; chloroform; 4: |Mitsunobu Displacement;
DOI:10.1016/j.bmc.2014.04.036