1-((Z)-(R)-4-Methyl-5-phenyl-pent-2-enylselanyl)-2-nitro-benzene

Base Information

• Chemical Name: 1-((Z)-(R)-4-Methyl-5-phenyl-pent-2-enylselanyl)-2-nitro-benzene
• CAS No.: 398136-80-6
• Molecular Formula: C₁₈H₁₉NO₂Se
• Molecular Weight: 360.314
• Mol file: 398136-80-6.mol

Synonyms:1-((Z)-(R)-4-Methyl-5-phenyl-pent-2-enylselanyl)-2-nitro-benzene

Chemical Property of 1-((Z)-(R)-4-Methyl-5-phenyl-pent-2-enylselanyl)-2-nitro-benzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-((Z)-(R)-4-Methyl-5-phenyl-pent-2-enylselanyl)-2-nitro-benzene

There total 1 articles about 1-((Z)-(R)-4-Methyl-5-phenyl-pent-2-enylselanyl)-2-nitro-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

ortho-nitrophenyl selenocyanate (51694-22-5) + (R)-3-methyl-4-phenylbutan-1-ol (34126-21-1) → 1-((Z)-(R)-4-Methyl-5-phenyl-pent-2-enylselanyl)-2-nitro-benzene (398136-80-6)

Guidance literature:

With tributylphosphine; In tetrahydrofuran;

DOI:10.1039/b006278m

Reference yield: 71.0%

1-((Z)-(R)-4-Methyl-5-phenyl-pent-2-enylselanyl)-2-nitro-benzene (398136-80-6) → (R)-4-Methyl-5-phenyl-pent-1-en-3-ol

Guidance literature:

1-((Z)-(R)-4-Methyl-5-phenyl-pent-2-enylselanyl)-2-nitro-benzene; With Cumene hydroperoxide; 4 A molecular sieve; vanadyl acetylacetonate; In dichloromethane; at -10 ℃; for 0.5h;

With tributylphosphine; In dichloromethane; at -10 ℃; for 0.0833333h;

DOI:10.1039/b316502g

Reference yield:

1-((Z)-(R)-4-Methyl-5-phenyl-pent-2-enylselanyl)-2-nitro-benzene (398136-80-6) → C18H19NO3Se

Guidance literature:

With Cumene hydroperoxide; 4 A molecular sieve; bis(acetylacetonate)oxovanadium; In dichloromethane; at -10 ℃; for 0.5h;

DOI:10.1039/b006278m

upstream raw materials:

ortho-nitrophenyl selenocyanate

(R)-3-methyl-4-phenylbutan-1-ol