C₃₀H₄₆N₄O₃SSi

Base Information

Chemical Name:C₃₀H₄₆N₄O₃SSi
CAS No.:1428343-07-0
Molecular Formula:C₃₀H₄₆N₄O₃SSi
Molecular Weight:570.872
Hs Code.:

C<sub>30</sub>H<sub>46</sub>N<sub>4</sub>O<sub>3</sub>SSi

Synonyms:C₃₀H₄₆N₄O₃SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₀H₄₆N₄O₃SSi

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Technology Process of C₃₀H₄₆N₄O₃SSi

There total 11 articles about C₃₀H₄₆N₄O₃SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1428343-04-7
C₂₃H₄₂O₄Si

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 1428343-07-0
C₃₀H₄₆N₄O₃SSi

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; toluene; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201206560

Reference yield:

: 1428342-96-4
C₁₂H₁₈O₃

: 1428343-07-0
C₃₀H₄₆N₄O₃SSi

Guidance literature:: Multi-step reaction with 6 steps

1.1: toluene / 17 h / 0 - 20 °C / Inert atmosphere

2.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 - 20 °C / Inert atmosphere

3.1: (-)-diisopinocamphenylborane chloride / tetrahydrofuran / 2.33 h / -30 - 20 °C / Inert atmosphere

4.1: 2,6-dimethylpyridine / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

5.1: camphor-10-sulfonic acid / dichloromethane; methanol / 0.5 h / 0 °C / Inert atmosphere

6.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 1 h / 0 - 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; oxalyl dichloride; camphor-10-sulfonic acid; dimethyl sulfoxide; triphenylphosphine; (-)-diisopinocamphenylborane chloride; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; toluene; 6.1: |Mitsunobu Displacement;
DOI:10.1002/anie.201206560

Reference yield:

: C₁₂H₂₆OSiZn

: 1428343-07-0
C₃₀H₄₆N₄O₃SSi

Guidance literature:: Multi-step reaction with 6 steps

1.1: toluene / 17 h / 0 - 20 °C / Inert atmosphere

2.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 - 20 °C / Inert atmosphere

3.1: (-)-diisopinocamphenylborane chloride / tetrahydrofuran / 2.33 h / -30 - 20 °C / Inert atmosphere

4.1: 2,6-dimethylpyridine / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

5.1: camphor-10-sulfonic acid / dichloromethane; methanol / 0.5 h / 0 °C / Inert atmosphere

6.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 1 h / 0 - 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; oxalyl dichloride; camphor-10-sulfonic acid; dimethyl sulfoxide; triphenylphosphine; (-)-diisopinocamphenylborane chloride; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; toluene; 6.1: |Mitsunobu Displacement;
DOI:10.1002/anie.201206560