2,3,4,5-Tetrachlorobenzoyl chloride

Base Information

Chemical Name:2,3,4,5-Tetrachlorobenzoyl chloride
CAS No.:42221-52-3
Molecular Formula:C7HCl5O
Molecular Weight:278.349
Hs Code.:2916399090
European Community (EC) Number:406-760-3,609-997-2
DSSTox Substance ID:DTXSID00420183
Nikkaji Number:J152.978A
Wikidata:Q72504739
Mol file:42221-52-3.mol

Synonyms:2,3,4,5-Tetrachlorobenzoylchloride;

Suppliers and Price of 2,3,4,5-Tetrachlorobenzoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TCI Chemical
2,3,4,5-Tetrachlorobenzoyl Chloride >98.0%(GC)(T)
25g
$ 95.00

American Custom Chemicals Corporation
2,3,4,5-TETRACHLOROBENZOYL CHLORIDE 95.00%
500G
$ 4412.10

American Custom Chemicals Corporation
2,3,4,5-TETRACHLOROBENZOYL CHLORIDE 95.00%
250G
$ 4273.50

Alichem
2,3,4,5-Tetrachlorobenzoyl Chloride
100g
$ 444.96

Total 55 raw suppliers

Chemical Property of 2,3,4,5-Tetrachlorobenzoyl chloride

Chemical Property:

Vapor Pressure:0.000695mmHg at 25°C
Melting Point:40 °C
Refractive Index:1.601
Boiling Point:308.1 °C at 760 mmHg
Flash Point:129.3 °C
PSA：17.07000
Density:1.7 g/cm³
LogP:4.67920
Solubility.:soluble in Toluene
XLogP3:4.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:277.844053
Heavy Atom Count:13
Complexity:209

Purity/Quality:

99% ^*data from raw suppliers

2,3,4,5-Tetrachlorobenzoyl Chloride >98.0%(GC)(T) ^*data from reagent suppliers

Safty Information:

Pictogram(s): C
Hazard Codes:C
Statements: 22-34-43
Safety Statements: 26-36/37/39-45

MSDS Files:

Useful:

Canonical SMILES:C1=C(C(=C(C(=C1Cl)Cl)Cl)Cl)C(=O)Cl

Technology Process of 2,3,4,5-Tetrachlorobenzoyl chloride

There total 3 articles about 2,3,4,5-Tetrachlorobenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.3%

: 50-74-8
2,3,4,5-tetrachlorobenzoic acid

: 2136-87-0
2,3,4,5-tetrachloro-1-(trichloromethyl)benzene

: 42221-52-3
2,3,4,5-tetrachlorobenzoyl chloride

Guidance literature:: With iron(III) oxide; at 155 ℃; for 2.2h; Autoclave;

Reference yield: 88.2%

: 50-74-8
2,3,4,5-tetrachlorobenzoic acid

: 42221-52-3
2,3,4,5-tetrachlorobenzoyl chloride

Guidance literature:: With bis(trichloromethyl) carbonate; triethylamine; for 7h; Time; Reflux;

Reference yield:

: 117-08-8
tetrachlorophthalic anhydride

: 42221-52-3
2,3,4,5-tetrachlorobenzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: water / 250 °C

2: thionyl chloride

With thionyl chloride; water;
DOI:10.1021/ja01203a036