1-O-acetyl-3-O-tert-butyldimethylsilyl-4,6-O-benzylidene-α-D-glucopyranose

Base Information

Chemical Name:1-O-acetyl-3-O-tert-butyldimethylsilyl-4,6-O-benzylidene-α-D-glucopyranose
CAS No.:1344087-26-8
Molecular Formula:C₂₁H₃₂O₇Si
Molecular Weight:424.566
Hs Code.:

Synonyms:1-O-acetyl-3-O-tert-butyldimethylsilyl-4,6-O-benzylidene-α-D-glucopyranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-O-acetyl-3-O-tert-butyldimethylsilyl-4,6-O-benzylidene-α-D-glucopyranose

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Technology Process of 1-O-acetyl-3-O-tert-butyldimethylsilyl-4,6-O-benzylidene-α-D-glucopyranose

There total 6 articles about 1-O-acetyl-3-O-tert-butyldimethylsilyl-4,6-O-benzylidene-α-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₃₄O₇Si

: 1344087-26-8
1-O-acetyl-3-O-tert-butyldimethylsilyl-4,6-O-benzylidene-α-D-glucopyranose

Guidance literature:: With hydrogenchloride; water; In dichloromethane; at 20 ℃; for 4h; silica gel; Inert atmosphere;
DOI:10.1016/j.carres.2011.08.008

Reference yield:

: C₂₂H₃₄O₇Si

: 1344087-26-8
1-O-acetyl-3-O-tert-butyldimethylsilyl-4,6-O-benzylidene-α-D-glucopyranose

Guidance literature:: With hydrogenchloride; water; In dichloromethane; at 20 ℃; for 0.5h; silica gel; Inert atmosphere;
DOI:10.1016/j.carres.2011.08.008

Reference yield:

: 23262-88-6,38081-45-7,38081-49-1,56193-00-1
O³-acetyl-O⁴,O⁶-((R)-benzylidene)-O¹,O²-((Ξ)-1-methoxy-ethylidene)-α-D-glucopyranose

: 1344087-26-8
1-O-acetyl-3-O-tert-butyldimethylsilyl-4,6-O-benzylidene-α-D-glucopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: methanol; sodium methylate / dichloromethane / 0 - 20 °C / Inert atmosphere

2: 1H-imidazole; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

3: hydrogenchloride; water / dichloromethane / 4 h / 20 °C / silica gel; Inert atmosphere

With 1H-imidazole; hydrogenchloride; methanol; water; sodium methylate; tetra-(n-butyl)ammonium iodide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2011.08.008