1,4-bis<5-(5-ethoxycarbonyl-2,4-dimethylpyrrol-3-yl)-5-oxopentyl>-2,3,5,6-tetramethylbenzene

Base Information

Chemical Name:1,4-bis<5-(5-ethoxycarbonyl-2,4-dimethylpyrrol-3-yl)-5-oxopentyl>-2,3,5,6-tetramethylbenzene
CAS No.:102410-88-8
Molecular Formula:C₃₈H₅₂N₂O₆
Molecular Weight:632.841
Hs Code.:

Synonyms:1,4-bis<5-(5-ethoxycarbonyl-2,4-dimethylpyrrol-3-yl)-5-oxopentyl>-2,3,5,6-tetramethylbenzene

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Chemical Property of 1,4-bis<5-(5-ethoxycarbonyl-2,4-dimethylpyrrol-3-yl)-5-oxopentyl>-2,3,5,6-tetramethylbenzene

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Technology Process of 1,4-bis<5-(5-ethoxycarbonyl-2,4-dimethylpyrrol-3-yl)-5-oxopentyl>-2,3,5,6-tetramethylbenzene

There total 12 articles about 1,4-bis<5-(5-ethoxycarbonyl-2,4-dimethylpyrrol-3-yl)-5-oxopentyl>-2,3,5,6-tetramethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 2199-44-2
3,5-dimethyl-2-ethoxycarbonyl-1H-pyrrole

: 102393-11-3
5-[4-(4-Chlorocarbonyl-butyl)-2,3,5,6-tetramethyl-phenyl]-pentanoyl chloride

: 102410-88-8
1,4-bis<5-(5-ethoxycarbonyl-2,4-dimethylpyrrol-3-yl)-5-oxopentyl>-2,3,5,6-tetramethylbenzene

Guidance literature:: With tin(IV) chloride; In nitromethane; dichloromethane;

Reference yield:

: 3022-16-0
1,4-bis(chloromethyl)-2,3,5,6-tetramethylbenzene

: 102410-88-8
1,4-bis<5-(5-ethoxycarbonyl-2,4-dimethylpyrrol-3-yl)-5-oxopentyl>-2,3,5,6-tetramethylbenzene

Guidance literature:: Multi-step reaction with 11 steps

1: 1.) Na / 1.) ethanol; 2.) ethanol, reflux, 0.5 h

2: H₂O, KOH / Heating

3: 94.7 percent / quinoline / 0.33 h / Heating

4: 89.4 percent / cc. H₂SO₄ / toluene

5: 89.6 percent / B₂H₆ / tetrahydrofuran

6: 91.2 percent / 48 percent HBr / H₂O / 0.5 h / Heating

7: 1.) Na / 1.) ethanol; 2.) ethanol, reflux

8: H₂O, KOH / Heating

9: 94.6 percent / quinoline / 0.33 h / Heating

10: SOCl₂ / Heating

11: SnCl₂ / CH₂Cl₂; nitromethane / 1 h / Ambient temperature

With quinoline; potassium hydroxide; thionyl chloride; sulfuric acid; water; hydrogen bromide; sodium; tin(ll) chloride; diborane; In tetrahydrofuran; nitromethane; dichloromethane; water; toluene;

Reference yield:

: 2004-70-8,17410-45-6,25212-15-1,64940-84-7
1-methylbuta-1,3-diene

: 102410-88-8
1,4-bis<5-(5-ethoxycarbonyl-2,4-dimethylpyrrol-3-yl)-5-oxopentyl>-2,3,5,6-tetramethylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: Zn, acetic acid

2: SnCl₂ / CH₂Cl₂; nitromethane / 1 h / Ambient temperature

With acetic acid; tin(ll) chloride; zinc; In nitromethane; dichloromethane;