11-{2,5-bis[(diethoxyphosphoryl)methyl]-4-methoxyphenoxy}undecyl acetate

Base Information

Chemical Name:11-{2,5-bis[(diethoxyphosphoryl)methyl]-4-methoxyphenoxy}undecyl acetate
CAS No.:443919-82-2
Molecular Formula:C₃₀H₅₄O₁₀P₂
Molecular Weight:636.7
Hs Code.:

Synonyms:11-{2,5-bis[(diethoxyphosphoryl)methyl]-4-methoxyphenoxy}undecyl acetate

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Chemical Property of 11-{2,5-bis[(diethoxyphosphoryl)methyl]-4-methoxyphenoxy}undecyl acetate

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Technology Process of 11-{2,5-bis[(diethoxyphosphoryl)methyl]-4-methoxyphenoxy}undecyl acetate

There total 4 articles about 11-{2,5-bis[(diethoxyphosphoryl)methyl]-4-methoxyphenoxy}undecyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 443919-81-1
11-[2,5-bis(bromomethyl)-4-methoxyphenoxy]undecyl acetate

: 122-52-1
triethyl phosphite

: 443919-82-2
11-{2,5-bis[(diethoxyphosphoryl)methyl]-4-methoxyphenoxy}undecyl acetate

Guidance literature:: at 160 ℃; for 8h;
DOI:10.1021/jp014675f

Reference yield:

: 1611-56-9
1-Bromo-11-hydroxyundecane

: 443919-82-2
11-{2,5-bis[(diethoxyphosphoryl)methyl]-4-methoxyphenoxy}undecyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 88.4 percent / NaH / tetrahydrofuran / 19 h / Heating

2: HBr / 30 h / 80 °C

3: 81 percent / 8 h / 160 °C

With hydrogen bromide; sodium hydride; In tetrahydrofuran;
DOI:10.1021/jp014675f

Reference yield:

: 150-76-5
4-methoxy-phenol

: 443919-82-2
11-{2,5-bis[(diethoxyphosphoryl)methyl]-4-methoxyphenoxy}undecyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 88.4 percent / NaH / tetrahydrofuran / 19 h / Heating

2: HBr / 30 h / 80 °C

3: 81 percent / 8 h / 160 °C

With hydrogen bromide; sodium hydride; In tetrahydrofuran;
DOI:10.1021/jp014675f