1,6-Dimethylphenanthrene

Base Information

• Chemical Name: 1,6-Dimethylphenanthrene
• CAS No.: 20291-74-1
• Molecular Formula: C₁₆H₁₄
• Molecular Weight: 206.287
• Hs Code.: 2902909090
• DSSTox Substance ID: DTXSID00942431
• Nikkaji Number: J957.762I
• Wikidata: Q82919444
• Mol file: 20291-74-1.mol

Synonyms:1,6-dimethylphenanthrene;20291-74-1;Phenanthrene, 1,6-dimethyl-;Phenanthrene,1,6-dimethyl-;1,6-Dimethyl-phenanthrene;1,6-Dimethylphenanthren;DTXSID00942431;YQMHHSZADKJARE-UHFFFAOYSA-N;F2167-9452

Chemical Property of 1,6-Dimethylphenanthrene

Chemical Property:

• Vapor Pressure: 2.49E-05mmHg at 25°C
• Refractive Index: 1.676
• Boiling Point: 369.6 °C at 760 mmHg
• Flash Point: 168.4 °C
• PSA: 0.00000
• Density: 1.084 g/cm³
• LogP: 4.60980
• XLogP3: 5.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 206.109550447
• Heavy Atom Count: 16
• Complexity: 244

Purity/Quality:

99% ^*data from raw suppliers

1,6-Dimethyl-phenanthrene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC2=C(C=C1)C=CC3=C(C=CC=C32)C
• Uses: 1,6-Dimethyl-phenanthrene is an environmental pollutant.

Technology Process of 1,6-Dimethylphenanthrene

There total 4 articles about 1,6-Dimethylphenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,6-dimethylcyclohexanone (2816-57-1) → 1,6-dimethylphenanthrene (20291-74-1)

Guidance literature:

With diethyl ether; at 0 ℃; Behandlung des gebildeten Alkohols mit wss. H₂SO₄ bei 0grad und Erhitzen des Reaktionsprodukts mit Selen auf 300-340grad;

Reference yield:

→ 1,6-dimethylphenanthrene (20291-74-1)

Guidance literature:

With hydrogenchloride; amalgamated zinc; Erhitzen des Reaktionsprodukts mit Selen auf 310grad bis 320grad;

Reference yield:

→ 1,6-dimethylphenanthrene (20291-74-1)

Guidance literature:

With potassium hydroxide; diethyl ether; sodium; Erhitzen mit P₂O₅ unter 6 mmHg Druck auf 135-140grad und anschliessendes Erhitzen mit Selen;

DOI:10.1039/jr9340000454

upstream raw materials:

2,6-dimethylcyclohexanone