C₁₅H₁₆F₃NO₂

Base Information

Chemical Name:C₁₅H₁₆F₃NO₂
CAS No.:1616505-88-4
Molecular Formula:C₁₅H₁₆F₃NO₂
Molecular Weight:299.293
Hs Code.:

C<sub>15</sub>H<sub>16</sub>F<sub>3</sub>NO<sub>2</sub>

Synonyms:C₁₅H₁₆F₃NO₂

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Chemical Property of C₁₅H₁₆F₃NO₂

Chemical Property:

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Technology Process of C₁₅H₁₆F₃NO₂

There total 5 articles about C₁₅H₁₆F₃NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106434-96-2
1-cyclopropyl-but-3-en-1-ol

: 1616505-88-4
C₁₅H₁₆F₃NO₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 21 °C

1.2: 5 - 58 °C

2.1: water; hydrogenchloride / tetrahydrofuran / 15.5 h / 20 - 40 °C

3.1: sodium acetate; hydroxylamine hydrochloride / ethanol; water / 1 h / 60 °C

4.1: sodium hypochlorite; triethylamine / water; dichloromethane / 19.5 - 22.8 °C

5.1: ChiralPAK? AS-H / methanol / Resolution of racemate

6.1: boron trifluoride diethyl etherate / toluene / 0.25 h / -78 °C

6.2: 1.5 h / -75 - -73 °C

With hydrogenchloride; sodium hypochlorite; boron trifluoride diethyl etherate; hydroxylamine hydrochloride; water; sodium acetate; sodium hydride; triethylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; mineral oil;

Reference yield:

: 1613394-10-7
[1-(2,2-diethoxyethoxy)but-3-en-1-yl]cyclopropane

: 1616505-88-4
C₁₅H₁₆F₃NO₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: water; hydrogenchloride / tetrahydrofuran / 15.5 h / 20 - 40 °C

2.1: sodium acetate; hydroxylamine hydrochloride / ethanol; water / 1 h / 60 °C

3.1: sodium hypochlorite; triethylamine / water; dichloromethane / 19.5 - 22.8 °C

4.1: ChiralPAK? AS-H / methanol / Resolution of racemate

5.1: boron trifluoride diethyl etherate / toluene / 0.25 h / -78 °C

5.2: 1.5 h / -75 - -73 °C

With hydrogenchloride; sodium hypochlorite; boron trifluoride diethyl etherate; hydroxylamine hydrochloride; water; sodium acetate; triethylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene;

Reference yield:

: 1613394-12-9
2-[(1-cyclopropylbut-3-en-1-yl)oxy]-N-hydroxyethanimine

: 1616505-88-4
C₁₅H₁₆F₃NO₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hypochlorite; triethylamine / water; dichloromethane / 19.5 - 22.8 °C

2.1: ChiralPAK? AS-H / methanol / Resolution of racemate

3.1: boron trifluoride diethyl etherate / toluene / 0.25 h / -78 °C

3.2: 1.5 h / -75 - -73 °C

With sodium hypochlorite; boron trifluoride diethyl etherate; triethylamine; In methanol; dichloromethane; water; toluene;