(4S,5R)-4-benzyloxymethyl-5-(2-bromo-1,1,2,2-tetrafluoroethyl)-2,2-dioxo-1,3,2-dioxathiolane

Base Information

Chemical Name:(4S,5R)-4-benzyloxymethyl-5-(2-bromo-1,1,2,2-tetrafluoroethyl)-2,2-dioxo-1,3,2-dioxathiolane
CAS No.:1050610-69-9
Molecular Formula:C₁₂H₁₁BrF₄O₅S
Molecular Weight:423.18
Hs Code.:

Synonyms:(4S,5R)-4-benzyloxymethyl-5-(2-bromo-1,1,2,2-tetrafluoroethyl)-2,2-dioxo-1,3,2-dioxathiolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S,5R)-4-benzyloxymethyl-5-(2-bromo-1,1,2,2-tetrafluoroethyl)-2,2-dioxo-1,3,2-dioxathiolane

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Technology Process of (4S,5R)-4-benzyloxymethyl-5-(2-bromo-1,1,2,2-tetrafluoroethyl)-2,2-dioxo-1,3,2-dioxathiolane

There total 1 articles about (4S,5R)-4-benzyloxymethyl-5-(2-bromo-1,1,2,2-tetrafluoroethyl)-2,2-dioxo-1,3,2-dioxathiolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: C₁₂H₁₁BrF₄O₄S

: 1050610-69-9
(4S,5R)-4-benzyloxymethyl-5-(2-bromo-1,1,2,2-tetrafluoroethyl)-2,2-dioxo-1,3,2-dioxathiolane

Guidance literature:: With tetrachloromethane; sodium periodate; ruthenium (III) chloride trihydrate; In water; acetonitrile; at 20 ℃; for 15h; Inert atmosphere;
DOI:10.1021/ol801272e

Reference yield: 68.0%

: 1050610-69-9
(4S,5R)-4-benzyloxymethyl-5-(2-bromo-1,1,2,2-tetrafluoroethyl)-2,2-dioxo-1,3,2-dioxathiolane

: 1050610-71-3
(3R,4R)-5-benzyloxy-1-bromo-1,1,2,2-tetrafluoropentane-3,4-diol

Guidance literature:: (4S,5R)-4-benzyloxymethyl-5-(2-bromo-1,1,2,2-tetrafluoroethyl)-2,2-dioxo-1,3,2-dioxathiolane; With ammonium formate; In N,N-dimethyl-formamide; at 80 ℃; for 6h; Inert atmosphere;

With sulfuric acid; In tetrahydrofuran; water; at 20 ℃; for 0.5h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol801272e