-2-methyl-3-(phenylthio)butan-1-ol

Base Information

• Chemical Name: -2-methyl-3-(phenylthio)butan-1-ol
• CAS No.: 136057-61-9
• Molecular Formula: C₁₁H₁₆OS
• Molecular Weight: 196.313

Synonyms:-2-methyl-3-(phenylthio)butan-1-ol

Chemical Property of -2-methyl-3-(phenylthio)butan-1-ol

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Technology Process of -2-methyl-3-(phenylthio)butan-1-ol

There total 17 articles about -2-methyl-3-(phenylthio)butan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

erythro-3-(2-methyl-1-oxo-3-(phenylthio)butyl)-2-oxazolidinone (137542-44-0,137542-45-1) → erythro-2-methyl-3-(phenylthio)butan-1-ol (136057-61-9,137623-79-1)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃; for 1h;

DOI:10.1021/jo00023a021

Reference yield: 88.0%

(S)-4-Isopropyl-3-((R)-2-methyl-3-phenylsulfanyl-butyryl)-oxazolidin-2-one → -2-methyl-3-(phenylthio)butan-1-ol (136057-61-9)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether;

DOI:10.1016/S0040-4020(96)01191-X

Reference yield: 71.0%

(S)-4-Isopropyl-3-((2R,3R)-2-methyl-3-phenylsulfanyl-butyryl)-oxazolidin-2-one (104320-00-5) → -2-methyl-3-(phenylthio)butan-1-ol (136057-61-9)

Guidance literature:

With lithium aluminium tetrahydride;

DOI:10.1016/0040-4039(91)80821-M

upstream raw materials:

(S)-4-Isopropyl-3-((2R,3R)-2-methyl-3-phenylsulfanyl-butyryl)-oxazolidin-2-one

(-)-(2S,3S)-methyl 2-methyl-3-phenylsulfanylbutanoate

methyl (E)-2-methyl-2-butenoate

2-(Trimethylsilyl)benzenethiol

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