allyl N-(-fluorenylmethoxycarbonyl)-3)>-L-serine

Base Information

Chemical Name:allyl N-(-fluorenylmethoxycarbonyl)-3)>-L-serine
CAS No.:155177-92-7
Molecular Formula:C₃₉H₄₀N₄O₁₁
Molecular Weight:740.767
Hs Code.:

allyl N-(-fluorenylmethoxycarbonyl)-<O-(2-azido-4,6-O-benzylidene-2-deoxy-3-O-levulinoyl-α-D-galactopyranosyl)-(1<*>3)>-L-serine

Synonyms:allyl N-(-fluorenylmethoxycarbonyl)-3)>-L-serine

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Chemical Property of allyl N-(-fluorenylmethoxycarbonyl)-3)>-L-serine

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Technology Process of allyl N-(-fluorenylmethoxycarbonyl)-3)>-L-serine

There total 5 articles about allyl N-(-fluorenylmethoxycarbonyl)-3)>-L-serine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 136497-85-3
N-(9-fluorenylmethoxycarbonyl)-L-serine allyl ester

: 155177-89-2
2-azido-4,6-O-benzylidene-2-deoxy-3-O-levulinoyl-β-D-galactopyranosyl fluoride

: allyl N-(9-fluorenylmethoxycarbonyl)-O-(2-azido-4,6-O-benzylidene-2-deoxy-3-O-levulinoyl-β-D-galactopyranosyl)-(1<*>3)-L-serine

: 155177-92-7
allyl N-(-fluorenylmethoxycarbonyl)-3)>-L-serine

Guidance literature:: With 4 A molecular sieve; Cp₂Zr(ClO₄)2; In dichloromethane;
DOI:10.1016/0040-4039(94)88332-7

Reference yield: 46.3%

: 136497-85-3
N-(9-fluorenylmethoxycarbonyl)-L-serine allyl ester

: 155177-88-1
2-azido-4,6-O-benzylidene-2-deoxy-3-O-levulinoyl-α-D-galactopyranosyl fluoride

: allyl N-(9-fluorenylmethoxycarbonyl)-O-(2-azido-4,6-O-benzylidene-2-deoxy-3-O-levulinoyl-β-D-galactopyranosyl)-(1<*>3)-L-serine

: 155177-92-7
allyl N-(-fluorenylmethoxycarbonyl)-3)>-L-serine

Guidance literature:: With 4 A molecular sieve; Cp₂Zr(ClO₄)2; In dichloromethane;
DOI:10.1016/0040-4039(94)88332-7

Reference yield:

: 2-azido-4,6-O-benzylidene-2-deoxy-3-O-levulinoyl-D-galactopyranose

: 155177-92-7
allyl N-(-fluorenylmethoxycarbonyl)-3)>-L-serine

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / diethylaminosulfur trifluoride / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 51.8 percent / AgClO₄, Cp₂ZrCl₂, 4A molecular sieves / CH₂Cl₂ / 36 h / -20 °C

With zirconocene dichloride; diethylamino-sulfur trifluoride; 4 A molecular sieve; silver perchlorate; In dichloromethane;
DOI:10.1016/0008-6215(94)00362-J