Sodium; benzotriazol-2-yl-(2-benzyloxycarbonylamino-acetylamino)-acetate

Base Information

Chemical Name:Sodium; benzotriazol-2-yl-(2-benzyloxycarbonylamino-acetylamino)-acetate
CAS No.:125453-29-4
Molecular Formula:C₁₈H₁₆N₅O₅*Na
Molecular Weight:405.345
Hs Code.:

Synonyms:Sodium; benzotriazol-2-yl-(2-benzyloxycarbonylamino-acetylamino)-acetate

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Chemical Property of Sodium; benzotriazol-2-yl-(2-benzyloxycarbonylamino-acetylamino)-acetate

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Technology Process of Sodium; benzotriazol-2-yl-(2-benzyloxycarbonylamino-acetylamino)-acetate

There total 2 articles about Sodium; benzotriazol-2-yl-(2-benzyloxycarbonylamino-acetylamino)-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 125453-28-3
Benzotriazol-1-yl-(2-benzyloxycarbonylamino-acetylamino)-acetic acid ethyl ester

: 125453-29-4
Sodium; benzotriazol-2-yl-(2-benzyloxycarbonylamino-acetylamino)-acetate

Guidance literature:: With sodium hydroxide; In diethyl ether; for 0.166667h;
DOI:10.1021/jo00294a042

Reference yield:

: 949-90-6
N-(carbobenzyloxy)glycinamide

: 125453-29-4
Sodium; benzotriazol-2-yl-(2-benzyloxycarbonylamino-acetylamino)-acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / p-TsOH*H₂O / toluene / 1.5 h / Heating

2: 42 percent / aq. NaOH / diethyl ether / 0.17 h

With sodium hydroxide; toluene-4-sulfonic acid; In diethyl ether; toluene;
DOI:10.1021/jo00294a042