C₄₂H₃₈N₂O₄

Base Information

Chemical Name:C₄₂H₃₈N₂O₄
CAS No.:1351204-74-4
Molecular Formula:C₄₂H₃₈N₂O₄
Molecular Weight:634.775
Hs Code.:

C<sub>42</sub>H<sub>38</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₄₂H₃₈N₂O₄

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Chemical Property of C₄₂H₃₈N₂O₄

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Technology Process of C₄₂H₃₈N₂O₄

There total 8 articles about C₄₂H₃₈N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1351204-63-1
C₃₄H₃₀N₂O₃

: 2746-25-0
p-Methoxybenzyl bromide

: 1351204-74-4
C₄₂H₃₈N₂O₄

Guidance literature:: C₃₄H₃₀N₂O₃; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.0833333h; Inert atmosphere;

p-Methoxybenzyl bromide; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja209244m

Reference yield:

: 120-72-9
indole

: 1351204-74-4
C₄₂H₃₈N₂O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: rhodium(II) acetate dimer / dichloromethane / 6 h / 20 °C / Inert atmosphere

2.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; 1-naphthalenecarboxylic acid; (1R,2R)-1,2-bis[(2-diphenylphosphanyl)benzoylamino]cyclohexane / tetrahydrofuran / 41 h / 20 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.08 h / 0 °C / Inert atmosphere

3.2: 2 h / 0 - 20 °C / Inert atmosphere

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; rhodium(II) acetate dimer; 1-naphthalenecarboxylic acid; sodium hydride; (1R,2R)-1,2-bis[(2-diphenylphosphanyl)benzoylamino]cyclohexane; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ja209244m

Reference yield:

: 1351204-98-2
C₂₃H₂₁N₃O₄S

: 1351204-74-4
C₄₂H₃₈N₂O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide / tetrahydrofuran; water / 3 h / 20 °C / Inert atmosphere

2.1: rhodium(II) acetate dimer / dichloromethane / 6 h / 20 °C / Inert atmosphere

3.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; 1-naphthalenecarboxylic acid; (1R,2R)-1,2-bis[(2-diphenylphosphanyl)benzoylamino]cyclohexane / tetrahydrofuran / 41 h / 20 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.08 h / 0 °C / Inert atmosphere

4.2: 2 h / 0 - 20 °C / Inert atmosphere

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; rhodium(II) acetate dimer; 1-naphthalenecarboxylic acid; sodium hydride; (1R,2R)-1,2-bis[(2-diphenylphosphanyl)benzoylamino]cyclohexane; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ja209244m