2-methoxy-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl trifluoromethanesulfonate

Base Information

Chemical Name:2-methoxy-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl trifluoromethanesulfonate
CAS No.:1437769-75-9
Molecular Formula:C₁₄H₁₈BF₃O₆S
Molecular Weight:382.166
Hs Code.:

Synonyms:2-methoxy-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl trifluoromethanesulfonate

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Chemical Property of 2-methoxy-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl trifluoromethanesulfonate

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Technology Process of 2-methoxy-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl trifluoromethanesulfonate

There total 1 articles about 2-methoxy-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90-05-1
2-methoxy-phenol

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1437769-75-9
2-methoxy-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: bis(1,5-cyclooctadiene)diiridium(I) dichloride; H₂SiEt₂ / benzene / 2 h / 20 °C / Inert atmosphere

1.2: 2 h / 20 - 80 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / -78 °C / Inert atmosphere

With bis(1,5-cyclooctadiene)diiridium(I) dichloride; H₂SiEt₂; N-ethyl-N,N-diisopropylamine; In dichloromethane; benzene;
DOI:10.1021/ol401140d

Reference yield:

: 1437769-75-9
2-methoxy-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl trifluoromethanesulfonate

: C₈H₈BF₃O₆S

Guidance literature:: 2-methoxy-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl trifluoromethanesulfonate; With sodium periodate; In tetrahydrofuran; water; at 20 ℃; for 0.5h; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1021/ol5031734

Reference yield:

: 1437769-75-9
2-methoxy-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl trifluoromethanesulfonate

: 2-methoxy-6-(1H-naphtho[1,8-de]-1,3,2-diazaborin-2(3H)-yl)phenyl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium periodate / tetrahydrofuran; water / 0.5 h / 20 °C / Inert atmosphere

1.2: 5 h / 20 °C / Inert atmosphere

2.1: dichloromethane / 0.5 h / 20 °C / Inert atmosphere; Molecular sieve

With sodium periodate; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ol5031734