Technology Process of C30H39N3O6S
There total 7 articles about C30H39N3O6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C28H32F3N3O7S2;
With
lithium hydroxide;
In
tetrahydrofuran; methanol; water;
at 20 ℃;
for 10h;
di-tert-butyl dicarbonate;
With
pyridine;
In
1,2-dichloro-ethane;
at 0 - 20 ℃;
for 10h;
With
hydrogenchloride;
In
diethyl ether; dichloromethane;
at 0 - 20 ℃;
for 1h;
- Guidance literature:
-
With
sodium hydroxide;
In
tetrahydrofuran; methanol; water;
at 20 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylamine / dichloromethane / 12 h / 0 - 20 °C
2: sodium t-butanolate / 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0) / toluene / 20 - 80 °C
3: hydroxylamine hydrochloride; sodium acetate / methanol / 20 °C
4: triethylamine / dichloromethane / 0 - 20 °C
5: sodium hydroxide / tetrahydrofuran; methanol; water / 3 h / 20 °C
With
sodium hydroxide; hydroxylamine hydrochloride; sodium acetate; triethylamine; sodium t-butanolate;
1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0);
In
tetrahydrofuran; methanol; dichloromethane; water; toluene;