N-T-BUTOXYCARBONYL-2-(TRIFLUOROMETHOXY)ANILINE

Base Information

Chemical Name:N-T-BUTOXYCARBONYL-2-(TRIFLUOROMETHOXY)ANILINE
CAS No.:561304-39-0
Molecular Formula:C12H14 F3 N O3
Molecular Weight:277.243
Hs Code.:
Mol file:561304-39-0.mol

Synonyms:Carbamicacid, [2-(trifluoromethoxy)phenyl]-, 1,1-dimethylethyl ester (9CI); (2-Trifluoromethoxyphenyl)carbamicacid tert-butyl ester

Suppliers and Price of N-T-BUTOXYCARBONYL-2-(TRIFLUOROMETHOXY)ANILINE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
tert-Butyl(2-(trifluoromethoxy)phenyl)carbamate 95+%
5g
$ 671.00

American Custom Chemicals Corporation
[2-(TRILUOROMETHOXY)PHENYL]-CARBAMIC ACID 1,1-DIMETHYL ETHYL ESTER 95.00%
1G
$ 945.95

Alichem
tert-Butyl(2-(trifluoromethoxy)phenyl)carbamate
1g
$ 400.00

Total 12 raw suppliers

Chemical Property of N-T-BUTOXYCARBONYL-2-(TRIFLUOROMETHOXY)ANILINE

Chemical Property:

Vapor Pressure:0.022mmHg at 25°C
Boiling Point:249.848°C at 760 mmHg
Flash Point:104.905°C
PSA：47.56000
Density:1.267g/cm³
LogP:4.00520
Storage Temp.:2-8°C

Purity/Quality:

99% ^*data from raw suppliers

tert-Butyl(2-(trifluoromethoxy)phenyl)carbamate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-T-BUTOXYCARBONYL-2-(TRIFLUOROMETHOXY)ANILINE

There total 1 articles about N-T-BUTOXYCARBONYL-2-(TRIFLUOROMETHOXY)ANILINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1535-75-7
2-trifluoromethoxy aniline

: 561304-39-0
tert-butyl N-[2-(trifluoromethoxy)phenyl]carbamate

Guidance literature:: In toluene; at 100 ℃; for 2h;
DOI:10.1021/jo0267798

Reference yield: 79.0%

: 124-38-9,18923-20-1
carbon dioxide

: 561304-39-0
tert-butyl N-[2-(trifluoromethoxy)phenyl]carbamate

: 561304-40-3
2-[(tert-butoxycarbonyl)amino]-3-(trifluoromethoxy)benzoic acid

Guidance literature:: tert-butyl N-[2-(trifluoromethoxy)phenyl]carbamate; With tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 - -50 ℃; for 1h;

carbon dioxide; In tetrahydrofuran; pentane;

With hydrogenchloride; In water; pH=1;

Reference yield: 46.0%

: 561304-39-0
tert-butyl N-[2-(trifluoromethoxy)phenyl]carbamate

: 1057720-33-8
tert-butyl N-[2-bromo-6-(trifluoromethoxy)phenyl]carbamate

Guidance literature:: tert-butyl N-[2-(trifluoromethoxy)phenyl]carbamate; With tert.-butyl lithium; In tetrahydrofuran; pentane; at -50 ℃; for 3h;

With carbon tetrabromide; In tetrahydrofuran; pentane; at -75 ℃; Further stages.;
DOI:10.1016/j.jfluchem.2007.09.003