2'-methoxy-4'-pentadecylacetophenone

Base Information

Chemical Name:2'-methoxy-4'-pentadecylacetophenone
CAS No.:852305-43-2
Molecular Formula:C₂₄H₄₀O₂
Molecular Weight:360.58
Hs Code.:

Synonyms:2'-methoxy-4'-pentadecylacetophenone

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Chemical Property of 2'-methoxy-4'-pentadecylacetophenone

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Technology Process of 2'-methoxy-4'-pentadecylacetophenone

There total 1 articles about 2'-methoxy-4'-pentadecylacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 52122-69-7
1-(2-hydroxy-4-pentadecylphenyl)ethanone

: 77-78-1
dimethyl sulfate

: 852305-43-2
2'-methoxy-4'-pentadecylacetophenone

Guidance literature:: With potassium hydroxide; In acetone; at 20 ℃; for 7h;
DOI:10.1246/bcsj.78.523

Reference yield: 91.0%

: 852305-43-2
2'-methoxy-4'-pentadecylacetophenone

: 702660-47-7
2-methoxy-4-pentadecylbenzoic acid

Guidance literature:: With sodium hypobromide; In 1,4-dioxane; at 20 ℃; for 20h;
DOI:10.1246/bcsj.78.523

Reference yield:

: 852305-43-2
2'-methoxy-4'-pentadecylacetophenone

: 4'-cyanobiphenyl-4-yl 2-methoxy-4-pentadecylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / sodium hypobromite / dioxane / 20 h / 20 °C

2: thionyl chloride / 4.5 h / 50 - 85 °C

3: 54 percent / Et₃N / CHCl₃ / 5 °C

With thionyl chloride; sodium hypobromide; triethylamine; In 1,4-dioxane; chloroform;
DOI:10.1246/bcsj.78.523