(1R,2S)-2-formylmethyl-1-(1-triphenylmethyl-1H-imidazol-4-yl)cyclopropane

Base Information

Chemical Name:(1R,2S)-2-formylmethyl-1-(1-triphenylmethyl-1H-imidazol-4-yl)cyclopropane
CAS No.:910630-36-3
Molecular Formula:C₂₇H₂₄N₂O
Molecular Weight:392.5
Hs Code.:

Synonyms:(1R,2S)-2-formylmethyl-1-(1-triphenylmethyl-1H-imidazol-4-yl)cyclopropane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2S)-2-formylmethyl-1-(1-triphenylmethyl-1H-imidazol-4-yl)cyclopropane

Chemical Property:

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Technology Process of (1R,2S)-2-formylmethyl-1-(1-triphenylmethyl-1H-imidazol-4-yl)cyclopropane

There total 2 articles about (1R,2S)-2-formylmethyl-1-(1-triphenylmethyl-1H-imidazol-4-yl)cyclopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-[2-(2-methoxy-vinyl)-cyclopropyl]-1-trityl-1H-imidazole

: 910630-36-3
(1R,2S)-2-formylmethyl-1-(1-triphenylmethyl-1H-imidazol-4-yl)cyclopropane

Guidance literature:: With hydrogenchloride; In acetone; at 20 ℃; for 0.00138889h;
DOI:10.1021/jm0603318

Reference yield:

: 250672-66-3
(1R,2R)-2-formyl-1-(1-triphenylmethyl-1H-imidazol-4-yl)cyclopropane

: 910630-36-3
(1R,2S)-2-formylmethyl-1-(1-triphenylmethyl-1H-imidazol-4-yl)cyclopropane

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaHMDS / tetrahydrofuran / 0.25 h / 0 °C

1.2: tetrahydrofuran / 3 h / 0 °C

2.1: 492 mg / aq. HCl / acetone / 0 h / 20 °C

With hydrogenchloride; sodium hexamethyldisilazane; In tetrahydrofuran; acetone; 1.2: Wittig reaction;
DOI:10.1021/jm0603318

Reference yield: 81.0%

: 910630-36-3
(1R,2S)-2-formylmethyl-1-(1-triphenylmethyl-1H-imidazol-4-yl)cyclopropane

: 681807-00-1
(1R,2S)-1-(1-triphenylmethyl-1H-imidazol-4-yl)-2-cyclopropaneacetic acid

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In water; tert-butyl alcohol; at 20 ℃; for 2h;
DOI:10.1021/jm0603318