2-(1-naphthyl)-1-phenylethanedione

Base Information

• Chemical Name: 2-(1-naphthyl)-1-phenylethanedione
• CAS No.: 16216-09-4
• Molecular Formula: C₁₈H₁₂O₂
• Molecular Weight: 260.292

Synonyms:2-(1-naphthyl)-1-phenylethanedione

Chemical Property of 2-(1-naphthyl)-1-phenylethanedione

Chemical Property:

Purity/Quality:

95%-98% ^*data from raw suppliers

Safty Information:

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Technology Process of 2-(1-naphthyl)-1-phenylethanedione

There total 41 articles about 2-(1-naphthyl)-1-phenylethanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-phenylethynyl-naphthalene (4044-57-9) → 2-(1-naphthyl)-1-phenylethanedione (16216-09-4)

Guidance literature:

With palladium dichloride; In dimethyl sulfoxide; at 130 ℃; for 24h; Inert atmosphere;

DOI:10.1021/ja103183r

Reference yield: 100.0%

1-(naphthalen-1-yl)-2-phenyl-2-(phenylimino)ethanone (1313850-11-1) → 2-(1-naphthyl)-1-phenylethanedione (16216-09-4)

Guidance literature:

With hydrogenchloride; water; In tetrahydrofuran; at 20 ℃; for 3h;

DOI:10.1016/j.tet.2011.04.020

Reference yield: 99.0%

5-hydroxy-N,N',5-triphenylimidazolidine-2,4-dione (1352131-39-5) + naphthalen-1-yl-lithium (14474-59-0) → 2-(1-naphthyl)-1-phenylethanedione (16216-09-4)

Guidance literature:

In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

DOI:10.1021/jo202304x

upstream raw materials:

1-(1-naphthyl)-2-phenylethanone

(2-Naphthalen-1-yl-[1,3]dithian-2-yl)-phenyl-methanone oxime

<(Benzoyloxy)-1-naphthylmethyl>triphenylphosphonium-chlorid

2-(naphthalen-1-yl)-1-phenylethan-1-one

Downstream raw materials:

[1]naphthyl-phenyl-ethanedione-2-hydrazone

(+/-)-hydroxy-phenyl-(naphthyl-⁽¹⁾)-acetic acid

2'--3'-phenyl-p-terphenyl

(S)-2-hydroxy-2-(naphthalen-1-yl)-1-phenylethanone

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