N-<4-Chlor-phenyl>-1-<4-chlor-phenyldithio>-formimid-saeure-aethylester

Base Information

• Chemical Name: N-<4-Chlor-phenyl>-1-<4-chlor-phenyldithio>-formimid-saeure-aethylester
• CAS No.: 109407-29-6
• Molecular Formula: C₁₅H₁₃Cl₂NOS₂
• Molecular Weight: 358.312
• Mol file: 109407-29-6.mol

Synonyms:N-<4-Chlor-phenyl>-1-<4-chlor-phenyldithio>-formimid-saeure-aethylester

Chemical Property of N-<4-Chlor-phenyl>-1-<4-chlor-phenyldithio>-formimid-saeure-aethylester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-<4-Chlor-phenyl>-1-<4-chlor-phenyldithio>-formimid-saeure-aethylester

There total 3 articles about N-<4-Chlor-phenyl>-1-<4-chlor-phenyldithio>-formimid-saeure-aethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Chlorophenyl isothiocyanate (2131-55-7) → N-<4-Chlor-phenyl>-1-<4-chlor-phenyldithio>-formimid-saeure-aethylester (109407-29-6)

Guidance literature:

Multi-step reaction with 2 steps

2: Py / benzene

With pyridine; In benzene;

DOI:10.1021/ja01486a036

Reference yield:

p-Chlorothiophenol (106-54-7) → N-<4-Chlor-phenyl>-1-<4-chlor-phenyldithio>-formimid-saeure-aethylester (109407-29-6)

Guidance literature:

Multi-step reaction with 2 steps

1: liquid sulphur dioxide / (chlorination)

2: Py / benzene

With pyridine; In benzene;

DOI:10.1021/ja01486a036

Reference yield:

O-ethyl N-(4-chlorophenyl)thiocarbamate (22001-51-0) + 4-chloro-benzenesulfenyl chloride (933-01-7) → N-<4-Chlor-phenyl>-1-<4-chlor-phenyldithio>-formimid-saeure-aethylester (109407-29-6)

Guidance literature:

With pyridine; In benzene;

DOI:10.1021/ja01486a036

upstream raw materials:

O-ethyl N-(4-chlorophenyl)thiocarbamate

4-chloro-benzenesulfenyl chloride

4-Chlorophenyl isothiocyanate

p-Chlorothiophenol