Technology Process of C18H24O5S
There total 7 articles about C18H24O5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium diisopropyl amide;
In
tetrahydrofuran;
1) -60 deg C, 10 min, 2) 0 deg C, 1 h, 3) r.t., 10 min;
DOI:10.1021/jo00299a052
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 99 percent / p-TsOH / benzene / 8 h / Heating
2: 99 percent / 3-chloroperoxybenzoic acid, NaHCO3 / CH2Cl2 / 4 h / Ambient temperature
3: 78 percent / LDA / tetrahydrofuran / 1) -60 deg C, 10 min, 2) 0 deg C, 1 h, 3) r.t., 10 min
With
sodium hydrogencarbonate; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane; benzene;
DOI:10.1021/jo00299a052
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1) LDA / THF, - 60 deg C, 1) 15 min, 2) 5 min
2: t-BuOK / 2-methyl-propan-2-ol; tetrahydrofuran / 0.17 h / Ambient temperature
3: 94 percent / LiClO4*3H2O, Bu3PO / toluene / 4.5 h / Heating
4: 99 percent / p-TsOH / benzene / 8 h / Heating
5: 99 percent / 3-chloroperoxybenzoic acid, NaHCO3 / CH2Cl2 / 4 h / Ambient temperature
6: 78 percent / LDA / tetrahydrofuran / 1) -60 deg C, 10 min, 2) 0 deg C, 1 h, 3) r.t., 10 min
With
Tributylphosphine oxide; potassium tert-butylate; lithium perchlorate; sodium hydrogencarbonate; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane; toluene; tert-butyl alcohol; benzene;
DOI:10.1021/jo00299a052
