C₅₈H₆₆N₉O₁₆P

Base Information

Chemical Name:C₅₈H₆₆N₉O₁₆P
CAS No.:246160-33-8
Molecular Formula:C₅₈H₆₆N₉O₁₆P
Molecular Weight:1176.19
Hs Code.:

C<sub>58</sub>H<sub>66</sub>N<sub>9</sub>O<sub>16</sub>P

Synonyms:C₅₈H₆₆N₉O₁₆P

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Chemical Property of C₅₈H₆₆N₉O₁₆P

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Technology Process of C₅₈H₆₆N₉O₁₆P

There total 9 articles about C₅₈H₆₆N₉O₁₆P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108549-23-1
Dibenzyl N,N-diisopropylphosphoramidite

: C₄₄H₅₃N₉O₁₃

: 246160-33-8
C₅₈H₆₆N₉O₁₆P

Guidance literature:: Dibenzyl N,N-diisopropylphosphoramidite; C₄₄H₅₃N₉O₁₃; With 1H-tetrazole; In dichloromethane; at 25 ℃; for 1h;

With 3-chloro-benzenecarboperoxoic acid; at -40 - 0 ℃; for 0.5h;
DOI:10.1021/jm990323+

Reference yield:

: 13726-52-8
diethyl N-(p-aminobenzoyl)-L-glutamate

: 246160-33-8
C₅₈H₆₆N₉O₁₆P

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium triacetoxyborohydride / CH₂Cl₂ / 4 h / 25 °C

2.1: NEt₃ / CH₂Cl₂ / 1 h / 25 °C

3.1: (PhCN)2PdCl₂; NEt₃ / acetonitrile / 8 h / 100 °C

4.1: NaOEt; EtOH / 1 h / 25 °C

5.1: tetrazole / CH₂Cl₂ / 1 h / 25 °C

5.2: MCPBA / 0.5 h / -40 - 0 °C

With 1H-tetrazole; bis(benzonitrile)palladium(II) dichloride; ethanol; sodium ethanolate; sodium tris(acetoxy)borohydride; triethylamine; In dichloromethane; acetonitrile; 1.1: reductive amination / 2.1: Acylation / 3.1: Substitution / 4.1: Deacetylation / 5.1: phosphorylation / 5.2: Oxidation;
DOI:10.1021/jm990323+

Reference yield:

: 1538-75-6
2,2-dimethylpropanoic anhydride

: 246160-33-8
C₅₈H₆₆N₉O₁₆P

Guidance literature:: Multi-step reaction with 7 steps

1.1: pyridine / 8 h / Heating

2.1: SeO₂ / dioxane / 3 h / 100 °C

3.1: sodium triacetoxyborohydride / CH₂Cl₂ / 4 h / 25 °C

4.1: NEt₃ / CH₂Cl₂ / 1 h / 25 °C

5.1: (PhCN)2PdCl₂; NEt₃ / acetonitrile / 8 h / 100 °C

6.1: NaOEt; EtOH / 1 h / 25 °C

7.1: tetrazole / CH₂Cl₂ / 1 h / 25 °C

7.2: MCPBA / 0.5 h / -40 - 0 °C

With pyridine; 1H-tetrazole; bis(benzonitrile)palladium(II) dichloride; selenium(IV) oxide; ethanol; sodium ethanolate; sodium tris(acetoxy)borohydride; triethylamine; In 1,4-dioxane; dichloromethane; acetonitrile; 1.1: Acylation / 2.1: Oxidation / 3.1: reductive amination / 4.1: Acylation / 5.1: Substitution / 6.1: Deacetylation / 7.1: phosphorylation / 7.2: Oxidation;
DOI:10.1021/jm990323+