ethyl 2-(4-(trifluoromethyl)phenyl)-2-nitroacetate

Base Information

Chemical Name:ethyl 2-(4-(trifluoromethyl)phenyl)-2-nitroacetate
CAS No.:1355333-04-8
Molecular Formula:C₁₁H₁₀F₃NO₄
Molecular Weight:277.2
Hs Code.:

Synonyms:ethyl 2-(4-(trifluoromethyl)phenyl)-2-nitroacetate

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Chemical Property of ethyl 2-(4-(trifluoromethyl)phenyl)-2-nitroacetate

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Technology Process of ethyl 2-(4-(trifluoromethyl)phenyl)-2-nitroacetate

There total 1 articles about ethyl 2-(4-(trifluoromethyl)phenyl)-2-nitroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 626-35-7
nitroacetic acid ethyl ester

: 402-43-7
p-trifluoromethylphenyl bromide

: 1355333-04-8
ethyl 2-(4-(trifluoromethyl)phenyl)-2-nitroacetate

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; cesium bicarbonate; tert-butyl XPhos; In toluene; at 75 - 80 ℃; for 18h; Inert atmosphere;
DOI:10.1021/ol203303b

Reference yield: 86.0%

: 1355333-04-8
ethyl 2-(4-(trifluoromethyl)phenyl)-2-nitroacetate

: 73790-06-4
ethyl 2-oxo-2-(4-(trifluoromethyl)phenyl)acetate

Guidance literature:: With potassium fluoride; tetrabutyl ammonium fluoride; methyl iodide; In tetrahydrofuran; at 20 ℃; for 16h; chemoselective reaction; Inert atmosphere;
DOI:10.1021/jo302071s