tetra-tert-butyl 2,2′,2″,2?-((2,2′-(2,2′-(((4-(4-sulfamoylphenoxy)-butyl)azanediyl)bis(methylene))bis(1H-imidazole-2,1-diyl))bis-(acetyl))bis(azanetriyl))tetraacetate

Base Information

Chemical Name:tetra-tert-butyl 2,2′,2″,2?-((2,2′-(2,2′-(((4-(4-sulfamoylphenoxy)-butyl)azanediyl)bis(methylene))bis(1H-imidazole-2,1-diyl))bis-(acetyl))bis(azanetriyl))tetraacetate
CAS No.:1417889-95-2
Molecular Formula:C₄₆H₇₀N₈O₁₃S
Molecular Weight:975.174
Hs Code.:

tetra-tert-butyl 2,2′,2″,2?-((2,2′-(2,2′-(((4-(4-sulfamoylphenoxy)-butyl)azanediyl)bis(methylene))bis(1H-imidazole-2,1-diyl))bis-(acetyl))bis(azanetriyl))tetraacetate

Synonyms:tetra-tert-butyl 2,2′,2″,2?-((2,2′-(2,2′-(((4-(4-sulfamoylphenoxy)-butyl)azanediyl)bis(methylene))bis(1H-imidazole-2,1-diyl))bis-(acetyl))bis(azanetriyl))tetraacetate

Suppliers and Price of tetra-tert-butyl 2,2′,2″,2?-((2,2′-(2,2′-(((4-(4-sulfamoylphenoxy)-butyl)azanediyl)bis(methylene))bis(1H-imidazole-2,1-diyl))bis-(acetyl))bis(azanetriyl))tetraacetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tetra-tert-butyl 2,2′,2″,2?-((2,2′-(2,2′-(((4-(4-sulfamoylphenoxy)-butyl)azanediyl)bis(methylene))bis(1H-imidazole-2,1-diyl))bis-(acetyl))bis(azanetriyl))tetraacetate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tetra-tert-butyl 2,2′,2″,2?-((2,2′-(2,2′-(((4-(4-sulfamoylphenoxy)-butyl)azanediyl)bis(methylene))bis(1H-imidazole-2,1-diyl))bis-(acetyl))bis(azanetriyl))tetraacetate

There total 2 articles about tetra-tert-butyl 2,2′,2″,2?-((2,2′-(2,2′-(((4-(4-sulfamoylphenoxy)-butyl)azanediyl)bis(methylene))bis(1H-imidazole-2,1-diyl))bis-(acetyl))bis(azanetriyl))tetraacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1228647-94-6
tert-butyl 2,2′-(2-(2-formyl-1H-imidazol-1-yl)-acetylazanediyl)diacetate

: 1446011-93-3
4-(4-sulfamoylphenoxy)butan-1-aminium2,2,2-trifluoroacetate

: 1417889-95-2
tetra-tert-butyl 2,2′,2″,2?-((2,2′-(2,2′-(((4-(4-sulfamoylphenoxy)-butyl)azanediyl)bis(methylene))bis(1H-imidazole-2,1-diyl))bis-(acetyl))bis(azanetriyl))tetraacetate

Guidance literature:: tert-butyl 2,2′-(2-(2-formyl-1H-imidazol-1-yl)-acetylazanediyl)diacetate; 4-(4-sulfamoylphenoxy)butan-1-aminium2,2,2-trifluoroacetate; With acetic acid; In 1,2-dichloro-ethane; at 75 ℃; for 0.5h; Inert atmosphere;

With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jm3015348

Reference yield:

: 1576-43-8
4-hydroxybenzenesulphonamide

: 1417889-95-2
tetra-tert-butyl 2,2′,2″,2?-((2,2′-(2,2′-(((4-(4-sulfamoylphenoxy)-butyl)azanediyl)bis(methylene))bis(1H-imidazole-2,1-diyl))bis-(acetyl))bis(azanetriyl))tetraacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetonitrile / 75 °C / Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere

3.1: acetic acid / 1,2-dichloro-ethane / 0.75 h / 75 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

With potassium carbonate; acetic acid; trifluoroacetic acid; In dichloromethane; 1,2-dichloro-ethane; acetonitrile;

Reference yield: 69.0%

: (NEt₄)2[rhenium(I)(bromide)3(carbonyl)3]

: 1417889-95-2
tetra-tert-butyl 2,2′,2″,2?-((2,2′-(2,2′-(((4-(4-sulfamoylphenoxy)-butyl)azanediyl)bis(methylene))bis(1H-imidazole-2,1-diyl))bis-(acetyl))bis(azanetriyl))tetraacetate

: 1417996-79-2
C₃₃H₃₈N₈O₁₆ReS⁽¹⁺⁾

Guidance literature:: (NEt₄)2[rhenium(I)(bromide)3(carbonyl)3]; tetra-tert-butyl 2,2′,2″,2?-((2,2′-(2,2′-(((4-(4-sulfamoylphenoxy)-butyl)azanediyl)bis(methylene))bis(1H-imidazole-2,1-diyl))bis-(acetyl))bis(azanetriyl))tetraacetate; In acetonitrile; at 90 ℃; for 4h; Inert atmosphere; Autoclave;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; Inert atmosphere;