N¹-benzyl-N⁴,N⁷,N¹⁰,N¹³-tetratosyl-1,4,7,10,13-pentaazacyclopentadecane

Base Information

Chemical Name:N¹-benzyl-N⁴,N⁷,N¹⁰,N¹³-tetratosyl-1,4,7,10,13-pentaazacyclopentadecane
CAS No.:164913-21-7
Molecular Formula:C₄₅H₅₅N₅O₈S₄
Molecular Weight:922.224
Hs Code.:

N<sup>1</sup>-benzyl-N<sup>4</sup>,N<sup>7</sup>,N<sup>10</sup>,N<sup>13</sup>-tetratosyl-1,4,7,10,13-pentaazacyclopentadecane

Synonyms:N¹-benzyl-N⁴,N⁷,N¹⁰,N¹³-tetratosyl-1,4,7,10,13-pentaazacyclopentadecane

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Chemical Property of N¹-benzyl-N⁴,N⁷,N¹⁰,N¹³-tetratosyl-1,4,7,10,13-pentaazacyclopentadecane

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Technology Process of N¹-benzyl-N⁴,N⁷,N¹⁰,N¹³-tetratosyl-1,4,7,10,13-pentaazacyclopentadecane

There total 3 articles about N¹-benzyl-N⁴,N⁷,N¹⁰,N¹³-tetratosyl-1,4,7,10,13-pentaazacyclopentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 112193-79-0
N³-benzyl-N¹,N⁵-ditosyl-3-aza-1,5-pentanediamine

: 132533-74-5
N,N'-bis(2-mesyloxyethyl)-N,N'-ditosyl-1,2-ethanediamine

: 164913-21-7
N¹-benzyl-N⁴,N⁷,N¹⁰,N¹³-tetratosyl-1,4,7,10,13-pentaazacyclopentadecane

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 96h;
DOI:10.1246/bcsj.73.693

Reference yield:

: 4556-90-5
N-(2-bromo-ethyl)-4-methyl-benzenesulfonamide

: 164913-21-7
N¹-benzyl-N⁴,N⁷,N¹⁰,N¹³-tetratosyl-1,4,7,10,13-pentaazacyclopentadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / sodium hydrogen carbonate / acetonitrile / 96 h / 70 °C

2: 36 percent / potassium carbonate / dimethylformamide / 96 h / 20 °C

With sodium hydrogencarbonate; potassium carbonate; In N,N-dimethyl-formamide; acetonitrile; 1: Alkylation / 2: Cyclization;
DOI:10.1246/bcsj.73.693

Reference yield:

: 100-46-9
benzylamine

: 164913-21-7
N¹-benzyl-N⁴,N⁷,N¹⁰,N¹³-tetratosyl-1,4,7,10,13-pentaazacyclopentadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / sodium hydrogen carbonate / acetonitrile / 96 h / 70 °C

2: 36 percent / potassium carbonate / dimethylformamide / 96 h / 20 °C

With sodium hydrogencarbonate; potassium carbonate; In N,N-dimethyl-formamide; acetonitrile; 1: Alkylation / 2: Cyclization;
DOI:10.1246/bcsj.73.693