Technology Process of 2,3-dichlorophenyl methoxymethyl ether
There total 1 articles about 2,3-dichlorophenyl methoxymethyl ether which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
acetonitrile;
at 50 - 60 ℃;
for 0.666667h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) butyl lithium, 2.) copper(I) iodide / 1.) hexane/Et2O, room temperature, 1 h, 2.) hexane/Et2O, room temperature, 30 min, 3.) hexane/Et2O, room temperature, 75 min
2: conc. H2SO4 / ethanol / 2 h / Heating
3: 89 percent / conc. H2SO4 / benzene / 0.5 h / Heating
With
copper(l) iodide; n-butyllithium; sulfuric acid;
In
ethanol; benzene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) butyl lithium, 2.) copper(I) iodide / 1.) hexane/Et2O, room temperature, 1 h, 2.) hexane/Et2O, room temperature, 30 min, 3.) hexane/Et2O, room temperature, 75 min
2: conc. H2SO4 / ethanol / 0.75 h / Heating
3: conc. H2SO4 / benzene / 0.5 h / Heating
With
copper(l) iodide; n-butyllithium; sulfuric acid;
In
ethanol; benzene;
