2-[1-hydroxy-4-trimethylsilyl-1-(3-trimethylsilyl-2-propynyl)-3-butynyl]phenol

Base Information

Chemical Name:2-[1-hydroxy-4-trimethylsilyl-1-(3-trimethylsilyl-2-propynyl)-3-butynyl]phenol
CAS No.:844857-41-6
Molecular Formula:C₁₉H₂₈O₂Si₂
Molecular Weight:344.601
Hs Code.:

Synonyms:2-[1-hydroxy-4-trimethylsilyl-1-(3-trimethylsilyl-2-propynyl)-3-butynyl]phenol

Suppliers and Price of 2-[1-hydroxy-4-trimethylsilyl-1-(3-trimethylsilyl-2-propynyl)-3-butynyl]phenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[1-hydroxy-4-trimethylsilyl-1-(3-trimethylsilyl-2-propynyl)-3-butynyl]phenol

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Technology Process of 2-[1-hydroxy-4-trimethylsilyl-1-(3-trimethylsilyl-2-propynyl)-3-butynyl]phenol

There total 1 articles about 2-[1-hydroxy-4-trimethylsilyl-1-(3-trimethylsilyl-2-propynyl)-3-butynyl]phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1433-61-0
2,2-dimethyl-4H-benzo[d][1,3]dioxin-4-one

: 123871-69-2
BrZnCH₂CCSi(CH₃)3

: 844857-41-6
2-[1-hydroxy-4-trimethylsilyl-1-(3-trimethylsilyl-2-propynyl)-3-butynyl]phenol

Guidance literature:: In tetrahydrofuran; at 20 ℃;
DOI:10.1002/anie.200460921

Reference yield: 78.0%

: 844857-41-6
2-[1-hydroxy-4-trimethylsilyl-1-(3-trimethylsilyl-2-propynyl)-3-butynyl]phenol

: 953780-74-0
2-[1-hydroxy-1-(2-propynyl)-3-butynyl]phenol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 15h;
DOI:10.1021/ja072571y

Reference yield:

: 844857-41-6
2-[1-hydroxy-4-trimethylsilyl-1-(3-trimethylsilyl-2-propynyl)-3-butynyl]phenol

: 844857-44-9
(E,E)-2-[1-hydroxy-4-phenyl-1-(3-phenyl-2-propenyl)-3-butenyl]phenol

Guidance literature:: Multi-step reaction with 3 steps

1: tetra-n-butylammonium fluoride trihydrate / tetrahydrofuran / 20 °C

2: CuI; Et₃N / Pd(PPh₃)2Cl₂

3: sodium bis(2-methoxyethoxy)aluminium hydride / tetrahydrofuran / 20 °C

With copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran;
DOI:10.1002/anie.200460921