N¹,N¹,N³,N³-tetrakis[2-(acetoxy)ethyl]5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)isophthalamide

Base Information

• Chemical Name: N¹,N¹,N³,N³-tetrakis[2-(acetoxy)ethyl]5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)isophthalamide
• CAS No.: 1041434-15-4
• Molecular Formula: C₃₀H₄₃BN₂O₁₂
• Molecular Weight: 634.489

Synonyms:N¹,N¹,N³,N³-tetrakis[2-(acetoxy)ethyl]5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)isophthalamide

Chemical Property of N¹,N¹,N³,N³-tetrakis[2-(acetoxy)ethyl]5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)isophthalamide

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Technology Process of N¹,N¹,N³,N³-tetrakis[2-(acetoxy)ethyl]5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)isophthalamide

There total 1 articles about N¹,N¹,N³,N³-tetrakis[2-(acetoxy)ethyl]5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)isophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-[(2-acetoxyethyl)amino]ethyl acetate (65121-95-1) + C14H15BCl2O4 → N1,N1,N3,N3-tetrakis[2-(acetoxy)ethyl]5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)isophthalamide (1041434-15-4)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1021/jo800736c

Reference yield: 49.0%

1,13-dibromo-8,8,18,18-tetramethylbacteriochlorin + N1,N1,N3,N3-tetrakis[2-(acetoxy)ethyl]5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)isophthalamide (1041434-15-4) → 3,13-bis[3,5-(bis(2-(acetoxy)ethyl)aminocarbonyl)phenyl]-8,8,18,18-tetramethylbacteriochlorin

Guidance literature:

With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; toluene; at 90 ℃;

DOI:10.1021/jo800736c

upstream raw materials:

2-[(2-acetoxyethyl)amino]ethyl acetate

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