Cyclohexanamine,4-(1-methylethyl)-, cis-

Base Information

Chemical Name:Cyclohexanamine,4-(1-methylethyl)-, cis-
CAS No.:23775-41-9
Molecular Formula:C₉H₁₉N
Molecular Weight:141.257
Hs Code.:
Mol file:23775-41-9.mol

Synonyms:Cyclohexylamine,4-isopropyl-, cis- (8CI); cis-4-Isopropylcyclohexanamine

Suppliers and Price of Cyclohexanamine,4-(1-methylethyl)-, cis-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
CIS-4-(1-METHYLETHYL)CYCLOHEXANAMINE 95.00%
5MG
$ 498.48

Total 6 raw suppliers

Chemical Property of Cyclohexanamine,4-(1-methylethyl)-, cis-

Chemical Property:

Boiling Point:185.6±8.0 °C(Predicted)
PKA:10.57±0.70(Predicted)
PSA：26.02000
Density:0.850±0.06 g/cm3(Predicted)
LogP:2.86020

Purity/Quality:

97% ^*data from raw suppliers

CIS-4-(1-METHYLETHYL)CYCLOHEXANAMINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclohexanamine,4-(1-methylethyl)-, cis-

There total 6 articles about Cyclohexanamine,4-(1-methylethyl)-, cis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 23775-42-0
trans-4-isopropylcyclohexylamine

: 23775-41-9
cis-4-isopropylcyclohexylamine

Guidance literature:: In methanol; at 20 ℃; for 16h; Molecular sieve;

With methanol; sodium tetrahydroborate; at 0 - 20 ℃; for 6h;

Reference yield:

: 5432-85-9
4-isopropyl-cyclohexanone

: 23775-41-9
cis-4-isopropylcyclohexylamine

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride; pyridine / ethanol / 5 h / Reflux

2: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Inert atmosphere; Reflux

With pyridine; lithium aluminium tetrahydride; hydroxylamine hydrochloride; In tetrahydrofuran; ethanol;
DOI:10.1021/acs.orglett.8b00929

Reference yield:

: 103027-46-9
4-Isopropylcyclohexanone oxime

: 23775-42-0
trans-4-isopropylcyclohexylamine

: 23775-41-9
cis-4-isopropylcyclohexylamine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 3h; diastereoselective reaction; Inert atmosphere; Reflux;
DOI:10.1021/acs.orglett.8b00929