tetradecanoic acid 4-[4-(2-dimethylamino-ethoxy)-phenyl]-3-hydroxy-3,4-diphenyl-1-tetradecanoyloxymethyl-butyl ester

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Chemical Name:tetradecanoic acid 4-[4-(2-dimethylamino-ethoxy)-phenyl]-3-hydroxy-3,4-diphenyl-1-tetradecanoyloxymethyl-butyl ester
CAS No.:286454-79-3
Molecular Formula:C₅₅H₈₅NO₆
Molecular Weight:856.283
Hs Code.:

Synonyms:tetradecanoic acid 4-[4-(2-dimethylamino-ethoxy)-phenyl]-3-hydroxy-3,4-diphenyl-1-tetradecanoyloxymethyl-butyl ester

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Chemical Property of tetradecanoic acid 4-[4-(2-dimethylamino-ethoxy)-phenyl]-3-hydroxy-3,4-diphenyl-1-tetradecanoyloxymethyl-butyl ester

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Technology Process of tetradecanoic acid 4-[4-(2-dimethylamino-ethoxy)-phenyl]-3-hydroxy-3,4-diphenyl-1-tetradecanoyloxymethyl-butyl ester

There total 7 articles about tetradecanoic acid 4-[4-(2-dimethylamino-ethoxy)-phenyl]-3-hydroxy-3,4-diphenyl-1-tetradecanoyloxymethyl-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6554-98-9
trans-4-Hydroxystilbene

: 286454-79-3
tetradecanoic acid 4-[4-(2-dimethylamino-ethoxy)-phenyl]-3-hydroxy-3,4-diphenyl-1-tetradecanoyloxymethyl-butyl ester

Guidance literature:: Multi-step reaction with 7 steps

1.1: 97 percent / KOH / dimethylformamide / 12 h / 25 °C

2.1: NBS; H₂O / dimethylsulfoxide / 0.5 h / 10 °C

2.2: 54 percent / aq. KOH / 0.5 h / 20 °C

3.1: 84 percent / CuI / 12 h / -40 - 20 °C

4.1: 75 percent / (CO)2Cl₂; DMSO; Et₃N / CH₂Cl₂ / -78 - 0 °C

5.1: 70 percent / diethyl ether / 12 h / -50 - 20 °C

6.1: OsO₄; NMO / acetone; H₂O / 20 °C

7.1: Et₃N; DMAP / CH₂Cl₂ / 12 h / 0 - 20 °C

With dmap; potassium hydroxide; N-Bromosuccinimide; osmium(VIII) oxide; N-methyl-2-indolinone; oxalyl dichloride; water; dimethyl sulfoxide; triethylamine; copper(l) iodide; In diethyl ether; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; 1.1: Alkylation / 2.1: Addition / 2.2: Elimination / 3.1: Grignard reaction / 4.1: Oxidation / 5.1: Grignard reaction / 6.1: Oxidation / 7.1: Acylation;
DOI:10.1016/S0040-4039(00)00421-4

Reference yield:

: 101717-72-0
(E)-N,N-dimethyl-2-(4-styrylphenoxy)ethanamine

: 286454-79-3
tetradecanoic acid 4-[4-(2-dimethylamino-ethoxy)-phenyl]-3-hydroxy-3,4-diphenyl-1-tetradecanoyloxymethyl-butyl ester

Guidance literature:: Multi-step reaction with 6 steps

1.1: NBS; H₂O / dimethylsulfoxide / 0.5 h / 10 °C

1.2: 54 percent / aq. KOH / 0.5 h / 20 °C

2.1: 84 percent / CuI / 12 h / -40 - 20 °C

3.1: 75 percent / (CO)2Cl₂; DMSO; Et₃N / CH₂Cl₂ / -78 - 0 °C

4.1: 70 percent / diethyl ether / 12 h / -50 - 20 °C

5.1: OsO₄; NMO / acetone; H₂O / 20 °C

6.1: Et₃N; DMAP / CH₂Cl₂ / 12 h / 0 - 20 °C

With dmap; N-Bromosuccinimide; osmium(VIII) oxide; N-methyl-2-indolinone; oxalyl dichloride; water; dimethyl sulfoxide; triethylamine; copper(l) iodide; In diethyl ether; dichloromethane; water; dimethyl sulfoxide; acetone; 1.1: Addition / 1.2: Elimination / 2.1: Grignard reaction / 3.1: Oxidation / 4.1: Grignard reaction / 5.1: Oxidation / 6.1: Acylation;
DOI:10.1016/S0040-4039(00)00421-4

Reference yield:

: Dimethyl-{2-[4-((2R,3R)-3-phenyl-oxiranyl)-phenoxy]-ethyl}-amine

: 286454-79-3
tetradecanoic acid 4-[4-(2-dimethylamino-ethoxy)-phenyl]-3-hydroxy-3,4-diphenyl-1-tetradecanoyloxymethyl-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 84 percent / CuI / 12 h / -40 - 20 °C

2: 75 percent / (CO)2Cl₂; DMSO; Et₃N / CH₂Cl₂ / -78 - 0 °C

3: 70 percent / diethyl ether / 12 h / -50 - 20 °C

4: OsO₄; NMO / acetone; H₂O / 20 °C

5: Et₃N; DMAP / CH₂Cl₂ / 12 h / 0 - 20 °C

With dmap; osmium(VIII) oxide; N-methyl-2-indolinone; oxalyl dichloride; dimethyl sulfoxide; triethylamine; copper(l) iodide; In diethyl ether; dichloromethane; water; acetone; 1: Grignard reaction / 2: Oxidation / 3: Grignard reaction / 4: Oxidation / 5: Acylation;
DOI:10.1016/S0040-4039(00)00421-4