Technology Process of C70H110N12O14
There total 4 articles about C70H110N12O14 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
for 16h;
DOI:10.1021/jo048630x
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium periodate / H2O; dimethylformamide; tetrahydrofuran / 16 h
2: 17 mg / NaCNBH3; trimethyl orthoformate; acetic acid / methanol / 16 h
With
sodium periodate; sodium cyanoborohydride; acetic acid; trimethyl orthoformate;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jo048630x
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 63 percent / PyBOP; HOBt; DiPEA / dimethylformamide / 16 h
2: sodium periodate / H2O; dimethylformamide; tetrahydrofuran / 16 h
3: 17 mg / NaCNBH3; trimethyl orthoformate; acetic acid / methanol / 16 h
With
sodium periodate; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; sodium cyanoborohydride; benzotriazol-1-ol; acetic acid; N-ethyl-N,N-diisopropylamine; trimethyl orthoformate;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jo048630x