1-[2-(cyclohexyloxy)-5-(4-formylphenyl)-3-thienyl]-2-(2-(cyclohexyloxy)-5-phenyl-3-thienyl)perfluorocyclopentene

Base Information

• Chemical Name: 1-[2-(cyclohexyloxy)-5-(4-formylphenyl)-3-thienyl]-2-(2-(cyclohexyloxy)-5-phenyl-3-thienyl)perfluorocyclopentene
• CAS No.: 950208-02-3
• Molecular Formula: C₃₈H₃₄F₆O₃S₂
• Molecular Weight: 716.809

Synonyms:1-[2-(cyclohexyloxy)-5-(4-formylphenyl)-3-thienyl]-2-(2-(cyclohexyloxy)-5-phenyl-3-thienyl)perfluorocyclopentene

Chemical Property of 1-[2-(cyclohexyloxy)-5-(4-formylphenyl)-3-thienyl]-2-(2-(cyclohexyloxy)-5-phenyl-3-thienyl)perfluorocyclopentene

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Technology Process of 1-[2-(cyclohexyloxy)-5-(4-formylphenyl)-3-thienyl]-2-(2-(cyclohexyloxy)-5-phenyl-3-thienyl)perfluorocyclopentene

There total 1 articles about 1-[2-(cyclohexyloxy)-5-(4-formylphenyl)-3-thienyl]-2-(2-(cyclohexyloxy)-5-phenyl-3-thienyl)perfluorocyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-(2-(cyclohexyloxy)-5-phenyl-3-thienyl)-2-{2-(cyclohexyloxy)-5-[4-([1,3]dioxolan-2-yl)-phenyl]-3-thienyl}perfluorocyclopentene (950208-01-2) → 1-[2-(cyclohexyloxy)-5-(4-formylphenyl)-3-thienyl]-2-(2-(cyclohexyloxy)-5-phenyl-3-thienyl)perfluorocyclopentene (950208-02-3)

Guidance literature:

With pyridinium p-toluenesulfonate; acetone; for 2h; Heating;

DOI:10.1016/j.tet.2008.05.088

Reference yield: 98.0%

1-[2-(cyclohexyloxy)-5-(4-formylphenyl)-3-thienyl]-2-(2-(cyclohexyloxy)-5-phenyl-3-thienyl)perfluorocyclopentene (950208-02-3) → 1-{2-(cyclohexyloxy)-5-[4-(hydroxymethyl)phenyl]-3-thienyl}-2-(2-(cyclohexyloxy)-5-phenyl-3-thienyl)perfluorocyclopentene (950208-03-4)

Guidance literature:

With potassium borohydride; In diethyl ether; ethanol; at 20 ℃; for 1h;

DOI:10.1016/j.tet.2008.05.088

upstream raw materials:

1-(2-(cyclohexyloxy)-5-phenyl-3-thienyl)-2-{2-(cyclohexyloxy)-5-[4-([1,3]dioxolan-2-yl)-phenyl]-3-thienyl}perfluorocyclopentene

Downstream raw materials:

1-{2-(cyclohexyloxy)-5-[4-(hydroxymethyl)phenyl]-3-thienyl}-2-(2-(cyclohexyloxy)-5-phenyl-3-thienyl)perfluorocyclopentene

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