10-phenyl-3-sulfanyl-5,10-dihydro-5λ⁶-benzo[e][1,2,4]triazolo[4,3-b][1,2,4]thiadiazine-5,5-dione

Base Information

• Chemical Name: 10-phenyl-3-sulfanyl-5,10-dihydro-5λ⁶-benzo[e][1,2,4]triazolo[4,3-b][1,2,4]thiadiazine-5,5-dione
• CAS No.: 1070676-29-7
• Molecular Formula: C₁₄H₁₀N₄O₂S₂
• Molecular Weight: 330.391

Synonyms:10-phenyl-3-sulfanyl-5,10-dihydro-5λ⁶-benzo[e][1,2,4]triazolo[4,3-b][1,2,4]thiadiazine-5,5-dione

Chemical Property of 10-phenyl-3-sulfanyl-5,10-dihydro-5λ⁶-benzo[e][1,2,4]triazolo[4,3-b][1,2,4]thiadiazine-5,5-dione

Chemical Property:

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Technology Process of 10-phenyl-3-sulfanyl-5,10-dihydro-5λ⁶-benzo[e][1,2,4]triazolo[4,3-b][1,2,4]thiadiazine-5,5-dione

There total 1 articles about 10-phenyl-3-sulfanyl-5,10-dihydro-5λ⁶-benzo[e][1,2,4]triazolo[4,3-b][1,2,4]thiadiazine-5,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

carbon disulfide (75-15-0,12122-00-8) + 3-hydrazino-4-phenyl-4H-1,2,4-benzothiadiazine 1,1-dioxide (107089-81-6) → 10-phenyl-3-sulfanyl-5,10-dihydro-5λ6-benzo[e][1,2,4]triazolo[4,3-b][1,2,4]thiadiazine-5,5-dione (1070676-29-7)

Guidance literature:

With potassium hydroxide; In ethanol; for 8h; Heating;

DOI:10.1016/j.bmc.2008.06.056

Reference yield: 86.0%

10-phenyl-3-sulfanyl-5,10-dihydro-5λ6-benzo[e][1,2,4]triazolo[4,3-b][1,2,4]thiadiazine-5,5-dione (1070676-29-7) + (2S)-N-[4-(5-bromopentyloxy)-5-methoxy-2-nitrobenzoyl]pyrrolidine-2-carboxaldehyde diethyl thioacetal (343308-57-6) → (2S)-N-{4-[5-[(10-phenyl-5,5-dioxo-5,10-dihydro-5-benzo[e][1,2,4]triazolo[4,3-b][1,2,4]thiadiazin-3-yl)sulfanyl]pentyloxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal (1070676-45-7)

Guidance literature:

With potassium carbonate; In acetone; Heating;

DOI:10.1016/j.bmc.2008.06.056

Reference yield: 85.0%

10-phenyl-3-sulfanyl-5,10-dihydro-5λ6-benzo[e][1,2,4]triazolo[4,3-b][1,2,4]thiadiazine-5,5-dione (1070676-29-7) + (2S)-N-[4-(4-bromobutyl)oxy-5-methoxy-2-nitrobenzoyl]pyrrolidine-2-carboxaldehyde diethylthioacetal (343308-56-5) → (2S)-N-{4-[4-[(10-phenyl-5,5-dioxo-5,10-dihydro-5-benzo[e][1,2,4]triazolo[4,3-b][1,2,4]thiadiazin-3-yl)sulfanyl]butoxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal (1070676-43-5)

Guidance literature:

With potassium carbonate; In acetone; Heating;

DOI:10.1016/j.bmc.2008.06.056

upstream raw materials:

carbon disulfide

3-hydrazino-4-phenyl-4H-1,2,4-benzothiadiazine 1,1-dioxide

Downstream raw materials:

(2S)-N-{4-[3-[(10-phenyl-5,5-dioxo-5,10-dihydro-5-benzo[e][1,2,4]triazolo[4,3-b][1,2,4]thiadiazin-3-yl)sulfanyl]propoxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal

(2S)-N-{4-[4-[(10-phenyl-5,5-dioxo-5,10-dihydro-5-benzo[e][1,2,4]triazolo[4,3-b][1,2,4]thiadiazin-3-yl)sulfanyl]butoxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal

(2S)-N-{4-[5-[(10-phenyl-5,5-dioxo-5,10-dihydro-5-benzo[e][1,2,4]triazolo[4,3-b][1,2,4]thiadiazin-3-yl)sulfanyl]pentyloxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal

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