(S)-3-butyn-2-ol hydrogen phthalate (S)-α-methylbenzylammonium salt

Base Information

Chemical Name:(S)-3-butyn-2-ol hydrogen phthalate (S)-α-methylbenzylammonium salt
CAS No.:100837-08-9
Molecular Formula:C₈H₁₁N*C₁₂H₁₀O₄
Molecular Weight:339.391
Hs Code.:

Synonyms:(S)-3-butyn-2-ol hydrogen phthalate (S)-α-methylbenzylammonium salt

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Chemical Property of (S)-3-butyn-2-ol hydrogen phthalate (S)-α-methylbenzylammonium salt

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Technology Process of (S)-3-butyn-2-ol hydrogen phthalate (S)-α-methylbenzylammonium salt

There total 5 articles about (S)-3-butyn-2-ol hydrogen phthalate (S)-α-methylbenzylammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 2627-86-3
(S)-1-phenyl-ethylamine

: 3113-93-7,3113-94-8,42969-62-0,100837-07-8
Phthalic acid mono-(1-methyl-prop-2-ynyl) ester

: 100837-08-9
(S)-3-butyn-2-ol hydrogen phthalate (S)-α-methylbenzylammonium salt

Guidance literature:: In acetone; for 0.5h; Heating;
DOI:10.1016/S0223-5234(99)80018-X

Reference yield:

: 85-44-9
phthalic anhydride

: 100837-08-9
(S)-3-butyn-2-ol hydrogen phthalate (S)-α-methylbenzylammonium salt

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / aq. NaOH / 0.08 h

2: acetone / 0.5 h / Heating

With sodium hydroxide; In acetone;
DOI:10.1021/jm00403a012

Reference yield:

: 85-44-9
phthalic anhydride

: 100837-08-9
(S)-3-butyn-2-ol hydrogen phthalate (S)-α-methylbenzylammonium salt

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / aq. NaOH / 0.08 h / 0 °C

2: 32 percent / acetone / 0.5 h / Heating

With sodium hydroxide; In acetone;
DOI:10.1016/S0223-5234(99)80018-X