4-amino-N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}butanamide

Base Information

Chemical Name:4-amino-N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}butanamide
CAS No.:921629-11-0
Molecular Formula:C₃₀H₃₂Cl₄N₂O₃
Molecular Weight:610.408
Hs Code.:

Synonyms:4-amino-N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}butanamide

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Chemical Property of 4-amino-N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}butanamide

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Technology Process of 4-amino-N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}butanamide

There total 10 articles about 4-amino-N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}butanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1056555-18-0
4-azido-N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}butanamide

: 921629-11-0
4-amino-N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}butanamide

Guidance literature:: With water; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 24h;

Reference yield:

: 1056555-58-8
ethyl 2-[4-(2-hydroxyethoxy)benzyl]pent-4-enoate

: 921629-11-0
4-amino-N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}butanamide

Guidance literature:: Multi-step reaction with 7 steps

1.1: tributylphosphine; 1,1'-azodicarbonyl-dipiperidine / toluene / 2 h / 80 °C

2.1: methanol; lithium hydroxide; water / tetrahydrofuran / 12 h / 50 °C

3.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 12 h / 20 °C

4.1: ozone / tetrahydrofuran; methanol / 0.33 h / -78 °C

4.2: 16 h / -78 - 20 °C

5.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.33 h / -78 - 0 °C

6.1: sodium azide / N,N-dimethyl-formamide / 24 h / 20 °C

7.1: water; triphenylphosphine / tetrahydrofuran / 24 h / 20 °C

With methanol; lithium hydroxide; sodium azide; tributylphosphine; water; ozone; N-ethyl-N,N-diisopropylamine; triphenylphosphine; HATU; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1056555-57-7
ethyl 2-[4-(2-{[tert-butyl(dimethyl)silyl]oxy}ethoxy)benzyl]pent-4-enoate

: 921629-11-0
4-amino-N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}butanamide

Guidance literature:: Multi-step reaction with 8 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

2.1: tributylphosphine; 1,1'-azodicarbonyl-dipiperidine / toluene / 2 h / 80 °C

3.1: methanol; lithium hydroxide; water / tetrahydrofuran / 12 h / 50 °C

4.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 12 h / 20 °C

5.1: ozone / tetrahydrofuran; methanol / 0.33 h / -78 °C

5.2: 16 h / -78 - 20 °C

6.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.33 h / -78 - 0 °C

7.1: sodium azide / N,N-dimethyl-formamide / 24 h / 20 °C

8.1: water; triphenylphosphine / tetrahydrofuran / 24 h / 20 °C

With methanol; lithium hydroxide; sodium azide; tributylphosphine; tetrabutyl ammonium fluoride; water; ozone; N-ethyl-N,N-diisopropylamine; triphenylphosphine; HATU; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;