3'-O-acetyl-N-(1-{[7-(diethylamino)-2-oxo-2H-chromen-4-yl]-methoxy}-2,2,6,6-tetramethylpiperidin-4-yl)-5'-O-(4,4'-dimethoxytrityl)-2'-deoxycytidine

Base Information

Chemical Name:3'-O-acetyl-N-(1-{[7-(diethylamino)-2-oxo-2H-chromen-4-yl]-methoxy}-2,2,6,6-tetramethylpiperidin-4-yl)-5'-O-(4,4'-dimethoxytrityl)-2'-deoxycytidine
CAS No.:1620751-85-0
Molecular Formula:C₅₅H₆₅N₅O₁₀
Molecular Weight:956.149
Hs Code.:

Synonyms:3'-O-acetyl-N-(1-{[7-(diethylamino)-2-oxo-2H-chromen-4-yl]-methoxy}-2,2,6,6-tetramethylpiperidin-4-yl)-5'-O-(4,4'-dimethoxytrityl)-2'-deoxycytidine

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Chemical Property of 3'-O-acetyl-N-(1-{[7-(diethylamino)-2-oxo-2H-chromen-4-yl]-methoxy}-2,2,6,6-tetramethylpiperidin-4-yl)-5'-O-(4,4'-dimethoxytrityl)-2'-deoxycytidine

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Technology Process of 3'-O-acetyl-N-(1-{[7-(diethylamino)-2-oxo-2H-chromen-4-yl]-methoxy}-2,2,6,6-tetramethylpiperidin-4-yl)-5'-O-(4,4'-dimethoxytrityl)-2'-deoxycytidine

There total 1 articles about 3'-O-acetyl-N-(1-{[7-(diethylamino)-2-oxo-2H-chromen-4-yl]-methoxy}-2,2,6,6-tetramethylpiperidin-4-yl)-5'-O-(4,4'-dimethoxytrityl)-2'-deoxycytidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1620751-84-9
4-[(4-amino-2,2,6,6-tetramethylpiperidin-1-yloxy)methyl]-7-(diethylamino)-2H-chromen-2-one

: C₄₇H₅₄N₂O₁₀S

: 1620751-85-0
3'-O-acetyl-N-(1-{[7-(diethylamino)-2-oxo-2H-chromen-4-yl]-methoxy}-2,2,6,6-tetramethylpiperidin-4-yl)-5'-O-(4,4'-dimethoxytrityl)-2'-deoxycytidine

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 19h;
DOI:10.1002/ejoc.201301692

Reference yield: 96.0%

: 1620751-85-0
3'-O-acetyl-N-(1-{[7-(diethylamino)-2-oxo-2H-chromen-4-yl]-methoxy}-2,2,6,6-tetramethylpiperidin-4-yl)-5'-O-(4,4'-dimethoxytrityl)-2'-deoxycytidine

: 1620751-86-1
N-(1-{[7-(diethylamino)-2-oxo-2H-chromen-4-yl]-methoxy}-2,2,6,6-tetramethylpiperidin-4-yl)-5'-O-(4,4'-dimethoxytrityl)-2'-deoxycytidine

Guidance literature:: With sodium hydrogencarbonate; In methanol; at 20 ℃; for 6h;
DOI:10.1002/ejoc.201301692

Reference yield:

: 1620751-85-0
3'-O-acetyl-N-(1-{[7-(diethylamino)-2-oxo-2H-chromen-4-yl]-methoxy}-2,2,6,6-tetramethylpiperidin-4-yl)-5'-O-(4,4'-dimethoxytrityl)-2'-deoxycytidine

: 1620751-87-2,1620751-88-3
C₆₂H₈₀N₇O₁₀P

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / methanol / 6 h / 20 °C

2: triethylamine / dichloromethane / 21 h / 20 °C

With sodium hydrogencarbonate; triethylamine; In methanol; dichloromethane;
DOI:10.1002/ejoc.201301692