isopropyl 4-(2-(4,6-di(2H₃)methoxypyrimidin-2-yloxy)benzylamino)benzoate

Base Information

Chemical Name:isopropyl 4-(2-(4,6-di(2H₃)methoxypyrimidin-2-yloxy)benzylamino)benzoate
CAS No.:1233862-13-9
Molecular Formula:C₂₃H₂₅N₃O₅
Molecular Weight:429.421
Hs Code.:

isopropyl 4-(2-(4,6-di(2H<sub>3</sub>)methoxypyrimidin-2-yloxy)benzylamino)benzoate

Synonyms:isopropyl 4-(2-(4,6-di(2H₃)methoxypyrimidin-2-yloxy)benzylamino)benzoate

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Chemical Property of isopropyl 4-(2-(4,6-di(2H₃)methoxypyrimidin-2-yloxy)benzylamino)benzoate

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Technology Process of isopropyl 4-(2-(4,6-di(2H₃)methoxypyrimidin-2-yloxy)benzylamino)benzoate

There total 5 articles about isopropyl 4-(2-(4,6-di(2H₃)methoxypyrimidin-2-yloxy)benzylamino)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1037629-82-5
4,6-di(2H₃)methoxy-2-(methylsulfonyl)pyrimidine

: isopropyl 4-(2-hydroxybenzylamino)benzoate

: 1233862-13-9
isopropyl 4-(2-(4,6-di(2H₃)methoxypyrimidin-2-yloxy)benzylamino)benzoate

Guidance literature:: With potassium carbonate; In acetonitrile; at 40 - 50 ℃; for 48h;
DOI:10.1002/jlcr.1749

Reference yield:

: 90-02-8
salicylaldehyde

: 1233862-13-9
isopropyl 4-(2-(4,6-di(2H₃)methoxypyrimidin-2-yloxy)benzylamino)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 1 h / 15 - 20 °C

2: sodium tetrahydroborate / methanol / 0.5 h / 0 - 5 °C

3: potassium carbonate / acetonitrile / 48 h / 40 - 50 °C

With sodium tetrahydroborate; potassium carbonate; In methanol; acetonitrile;
DOI:10.1002/jlcr.1749

Reference yield:

: 4,6-di(2H₃)methoxy-2-(methylthio)pyrimidine

: 1233862-13-9
isopropyl 4-(2-(4,6-di(2H₃)methoxypyrimidin-2-yloxy)benzylamino)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tungstate; urea hydrogen peroxide adduct / acetic acid / 4 h / 50 °C

2: potassium carbonate / acetonitrile / 48 h / 40 - 50 °C

With sodium tungstate; urea hydrogen peroxide adduct; potassium carbonate; In acetic acid; acetonitrile;
DOI:10.1002/jlcr.1749