2-(2-Benzo[1,3]dioxol-5-yl-[1,3]dioxolan-2-yl)-1-[4-(tert-butyl-diphenyl-silanyloxy)-2,6-dimethoxy-3-(3-methyl-but-2-enyl)-phenyl]-ethanol

Base Information

Chemical Name:2-(2-Benzo[1,3]dioxol-5-yl-[1,3]dioxolan-2-yl)-1-[4-(tert-butyl-diphenyl-silanyloxy)-2,6-dimethoxy-3-(3-methyl-but-2-enyl)-phenyl]-ethanol
CAS No.:191677-51-7
Molecular Formula:C₄₁H₄₈O₈Si
Molecular Weight:696.913
Hs Code.:

Synonyms:2-(2-Benzo[1,3]dioxol-5-yl-[1,3]dioxolan-2-yl)-1-[4-(tert-butyl-diphenyl-silanyloxy)-2,6-dimethoxy-3-(3-methyl-but-2-enyl)-phenyl]-ethanol

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Chemical Property of 2-(2-Benzo[1,3]dioxol-5-yl-[1,3]dioxolan-2-yl)-1-[4-(tert-butyl-diphenyl-silanyloxy)-2,6-dimethoxy-3-(3-methyl-but-2-enyl)-phenyl]-ethanol

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Technology Process of 2-(2-Benzo[1,3]dioxol-5-yl-[1,3]dioxolan-2-yl)-1-[4-(tert-butyl-diphenyl-silanyloxy)-2,6-dimethoxy-3-(3-methyl-but-2-enyl)-phenyl]-ethanol

There total 9 articles about 2-(2-Benzo[1,3]dioxol-5-yl-[1,3]dioxolan-2-yl)-1-[4-(tert-butyl-diphenyl-silanyloxy)-2,6-dimethoxy-3-(3-methyl-but-2-enyl)-phenyl]-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 191677-85-7
(2-Benzo[1,3]dioxol-5-yl-[1,3]dioxolan-2-yl)-acetaldehyde

: 191677-46-0
tert-Butyl-[3,5-dimethoxy-2-(3-methyl-but-2-enyl)-phenoxy]-diphenyl-silane

: 191677-51-7
2-(2-Benzo[1,3]dioxol-5-yl-[1,3]dioxolan-2-yl)-1-[4-(tert-butyl-diphenyl-silanyloxy)-2,6-dimethoxy-3-(3-methyl-but-2-enyl)-phenyl]-ethanol

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at -78 ℃;
DOI:10.1016/S0040-4039(97)00927-1

Reference yield:

: 500-99-2
3,5-dimethoxyphenol

: 191677-51-7
2-(2-Benzo[1,3]dioxol-5-yl-[1,3]dioxolan-2-yl)-1-[4-(tert-butyl-diphenyl-silanyloxy)-2,6-dimethoxy-3-(3-methyl-but-2-enyl)-phenyl]-ethanol

Guidance literature:: Multi-step reaction with 3 steps

1: 30 percent / NaH / tetrahydrofuran / 25 °C

2: 80 percent / imidazole / dimethylformamide / 25 °C

3: 61 percent / BuLi / tetrahydrofuran / -78 °C

With 1H-imidazole; n-butyllithium; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(97)00927-1

Reference yield:

: 120-57-0,30024-74-9
piperonal

: 191677-51-7
2-(2-Benzo[1,3]dioxol-5-yl-[1,3]dioxolan-2-yl)-1-[4-(tert-butyl-diphenyl-silanyloxy)-2,6-dimethoxy-3-(3-methyl-but-2-enyl)-phenyl]-ethanol

Guidance literature:: Multi-step reaction with 6 steps

1: 86 percent / tetrahydrofuran / -78 °C

2: 60 percent / PCC / CH₂Cl₂ / 25 °C

3: 43 percent / p-TsOH / benzene / Heating

4: 73 percent / LiAlH₄ / diethyl ether / 25 °C

5: 58 percent / PCC / CH₂Cl₂ / 25 °C

6: 61 percent / BuLi / tetrahydrofuran / -78 °C

With lithium aluminium tetrahydride; n-butyllithium; toluene-4-sulfonic acid; pyridinium chlorochromate; In tetrahydrofuran; diethyl ether; dichloromethane; benzene;
DOI:10.1016/S0040-4039(97)00927-1