2-chloro-4-methoxy-1-{[1-methyl-5-(2-naphthylmethoxy)pyrazole-4-yl]carbonyl}-3-(1-oxothianylideneamino)benzene

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Chemical Name:2-chloro-4-methoxy-1-{[1-methyl-5-(2-naphthylmethoxy)pyrazole-4-yl]carbonyl}-3-(1-oxothianylideneamino)benzene
CAS No.:1207341-29-4
Molecular Formula:C₂₈H₂₈ClN₃O₄S
Molecular Weight:538.067
Hs Code.:

Synonyms:2-chloro-4-methoxy-1-{[1-methyl-5-(2-naphthylmethoxy)pyrazole-4-yl]carbonyl}-3-(1-oxothianylideneamino)benzene

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Chemical Property of 2-chloro-4-methoxy-1-{[1-methyl-5-(2-naphthylmethoxy)pyrazole-4-yl]carbonyl}-3-(1-oxothianylideneamino)benzene

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Technology Process of 2-chloro-4-methoxy-1-{[1-methyl-5-(2-naphthylmethoxy)pyrazole-4-yl]carbonyl}-3-(1-oxothianylideneamino)benzene

There total 2 articles about 2-chloro-4-methoxy-1-{[1-methyl-5-(2-naphthylmethoxy)pyrazole-4-yl]carbonyl}-3-(1-oxothianylideneamino)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 1207341-28-3
2-chloro-1-[(5-hydroxy-1-methylpyrazole-4-yl)carbonyl]-4-methoxy-3-(1-oxothianylideneamino)benzene

: 939-26-4
2-bromomethylnaphthyl bromide

: 1207341-29-4
2-chloro-4-methoxy-1-{[1-methyl-5-(2-naphthylmethoxy)pyrazole-4-yl]carbonyl}-3-(1-oxothianylideneamino)benzene

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

Reference yield:

: 1207343-99-4
2-chloro-4-methoxy-3-(1-oxothianylideneamino)benzoic acid

: 1207341-29-4
2-chloro-4-methoxy-1-{[1-methyl-5-(2-naphthylmethoxy)pyrazole-4-yl]carbonyl}-3-(1-oxothianylideneamino)benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,1'-carbonyldiimidazole / chloroform / 1 h / 20 °C

1.2: 1 h / Reflux

1.3: 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

With potassium carbonate; 1,1'-carbonyldiimidazole; In chloroform; N,N-dimethyl-formamide;