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{(C5H4C(C6H5)3)Fe(CO)2}2

Base Information
  • Chemical Name:{(C5H4C(C6H5)3)Fe(CO)2}2
  • CAS No.:138697-88-8
  • Molecular Formula:C52H38Fe2O4
  • Molecular Weight:838.565
  • Hs Code.:
{(C<sub>5</sub>H<sub>4</sub>C(C<sub>6</sub>H<sub>5</sub>)3)Fe(CO)2}2

Synonyms:{(C5H4C(C6H5)3)Fe(CO)2}2

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Chemical Property of {(C5H4C(C6H5)3)Fe(CO)2}2
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Technology Process of {(C5H4C(C6H5)3)Fe(CO)2}2

There total 1 articles about {(C5H4C(C6H5)3)Fe(CO)2}2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In n-heptane; diethylene glycol; solution deoxygenated, heated (120°C, under N2, 24 h), black solution, cooled in ice; filtered, more product on refrigeration of mother liquor;
Guidance literature:
With iodine; In hexane; dichloromethane; benzene; under N2, room temperature, iodine soln. added dropwise to the stirred solution of the complex, monitored by IR (2 h); excess iodine removed by aq. Na2S2O3, organic layer separated, dried (MgSO4), solvent removed in vac., column chromatography (silica gel/hexane slurry/benzene eluent);
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